(S)-2-(pyrrol-1-yl)-pentanedioic acid 1-benzyl ester 5-((S)-2,6-di(pyrrol-1-yl)-hexyl) ester

Base Information

Chemical Name:(S)-2-(pyrrol-1-yl)-pentanedioic acid 1-benzyl ester 5-((S)-2,6-di(pyrrol-1-yl)-hexyl) ester
CAS No.:1346772-47-1
Molecular Formula:C₃₀H₃₅N₃O₄
Molecular Weight:501.626
Hs Code.:

Synonyms:(S)-2-(pyrrol-1-yl)-pentanedioic acid 1-benzyl ester 5-((S)-2,6-di(pyrrol-1-yl)-hexyl) ester

Suppliers and Price of (S)-2-(pyrrol-1-yl)-pentanedioic acid 1-benzyl ester 5-((S)-2,6-di(pyrrol-1-yl)-hexyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-2-(pyrrol-1-yl)-pentanedioic acid 1-benzyl ester 5-((S)-2,6-di(pyrrol-1-yl)-hexyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-2-(pyrrol-1-yl)-pentanedioic acid 1-benzyl ester 5-((S)-2,6-di(pyrrol-1-yl)-hexyl) ester

There total 4 articles about (S)-2-(pyrrol-1-yl)-pentanedioic acid 1-benzyl ester 5-((S)-2,6-di(pyrrol-1-yl)-hexyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 866139-30-2
(S)-2-pyrrol-1-yl-pentanedioic acid 1-benzyl ester

: 1346772-50-6
2,6-di(pyrrol-1-yl)-hexan-1-ol

: 1346772-47-1
(S)-2-(pyrrol-1-yl)-pentanedioic acid 1-benzyl ester 5-((S)-2,6-di(pyrrol-1-yl)-hexyl) ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.10.047

Reference yield:

: 13030-09-6
1-benzyl L-glutamate

: 1346772-47-1
(S)-2-(pyrrol-1-yl)-pentanedioic acid 1-benzyl ester 5-((S)-2,6-di(pyrrol-1-yl)-hexyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate; acetic acid / water / 2 h / 75 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 3 h / 20 °C / Inert atmosphere

With dmap; sodium acetate; acetic acid; dicyclohexyl-carbodiimide; In dichloromethane; water; 1: Clauson-Kaas reaction;
DOI:10.1016/j.tetlet.2011.10.047

Reference yield:

: 687-64-9
L-lysine methyl ester

: 1346772-47-1
(S)-2-(pyrrol-1-yl)-pentanedioic acid 1-benzyl ester 5-((S)-2,6-di(pyrrol-1-yl)-hexyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate; acetic acid / water / 2 h / 75 °C

2: lithium aluminium tetrahydride / diethyl ether / 0 °C / Inert atmosphere

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 3 h / 20 °C / Inert atmosphere

With dmap; lithium aluminium tetrahydride; sodium acetate; acetic acid; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane; water; 1: Clauson-Kaas reaction;
DOI:10.1016/j.tetlet.2011.10.047