4-(6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)quinoxalin-2-yl)-N,N-dimethylaniline

Base Information

Chemical Name:4-(6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)quinoxalin-2-yl)-N,N-dimethylaniline
CAS No.:1437281-39-4
Molecular Formula:C₂₄H₃₃N₃O₂Si
Molecular Weight:423.63
Hs Code.:

Synonyms:4-(6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)quinoxalin-2-yl)-N,N-dimethylaniline

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Chemical Property of 4-(6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)quinoxalin-2-yl)-N,N-dimethylaniline

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Technology Process of 4-(6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)quinoxalin-2-yl)-N,N-dimethylaniline

There total 3 articles about 4-(6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)quinoxalin-2-yl)-N,N-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1437281-38-3
6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)-2-chloroquinoxaline

: 171364-78-6
(4-(N,N-dimethylamino)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1437281-39-4
4-(6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)quinoxalin-2-yl)-N,N-dimethylaniline

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; for 3h; Reflux;
DOI:10.1021/ml4000707

Reference yield:

: 55687-04-2
6-hydroxy-2-chloroquinoxaline

: 1437281-39-4
4-(6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)quinoxalin-2-yl)-N,N-dimethylaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 80 °C

1.2: 2.5 h / 80 °C

2.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; toluene; ethanol / 3 h / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ml4000707

Reference yield:

: 55687-11-1
6-methoxy-2-chloroquinoxaline

: 1437281-39-4
4-(6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)quinoxalin-2-yl)-N,N-dimethylaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride / toluene / 4 h / 0 - 80 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 80 °C

2.2: 2.5 h / 80 °C

3.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; toluene; ethanol / 3 h / Reflux

With aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ml4000707