phosphoric acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Base Information

Chemical Name:phosphoric acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester
CAS No.:765299-11-4
Molecular Formula:C₃₁H₄₇NO₁₂P₂
Molecular Weight:687.661
Hs Code.:

phosphoric acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Synonyms:phosphoric acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

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Chemical Property of phosphoric acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

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Technology Process of phosphoric acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

There total 3 articles about phosphoric acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 765299-10-3
phosphorous acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphanyloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

: 765299-11-4
phosphoric acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Guidance literature:: With urea hydrogen peroxide; In toluene; at 20 ℃;
DOI:10.1023/B:RUGC.0000016014.90042.3b

Reference yield:

: 64505-22-2
1,2-O-isopropylideneglycero-3-(benzyldiethylphosphoramidite)

: 765299-11-4
phosphoric acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 10 h / 90 °C / 500 Torr

2: 0.58 g / urea hydrogen peroxide adduct / toluene / 20 °C

With urea hydrogen peroxide; In toluene;
DOI:10.1023/B:RUGC.0000016014.90042.3b

Reference yield:

: 105-59-9
N-Methyldiethanolamine

: 765299-11-4
phosphoric acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 10 h / 90 °C / 500 Torr

2: 0.58 g / urea hydrogen peroxide adduct / toluene / 20 °C

With urea hydrogen peroxide; In toluene;
DOI:10.1023/B:RUGC.0000016014.90042.3b