phosphorous acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphanyloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Base Information

• Chemical Name: phosphorous acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphanyloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester
• CAS No.: 765299-10-3
• Molecular Formula: C₃₁H₄₇NO₁₀P₂
• Molecular Weight: 655.662

Synonyms:

Chemical Property of phosphorous acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphanyloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Chemical Property:

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Safty Information:

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Useful:

Technology Process of phosphorous acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphanyloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

There total 1 articles about phosphorous acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphanyloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-O-isopropylideneglycero-3-(benzyldiethylphosphoramidite) (64505-22-2) + N-Methyldiethanolamine (105-59-9) → phosphorous acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphanyloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester (765299-10-3)

Guidance literature:

In toluene; at 90 ℃; for 10h; under 500 Torr;

DOI:10.1023/B:RUGC.0000016014.90042.3b

Reference yield:

phosphorous acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphanyloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester (765299-10-3) → phosphoric acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester (765299-11-4)

Guidance literature:

With urea hydrogen peroxide; In toluene; at 20 ℃;

DOI:10.1023/B:RUGC.0000016014.90042.3b

Reference yield:

phosphorous acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphanyloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester (765299-10-3) → thiophosphoric acid O-benzyl ester O'-[2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-thiophosphoryloxy]-ethyl}-methyl-amino)-ethyl] ester O''-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl) ester (765299-12-5)

Guidance literature:

With sulfur; In toluene; at 20 ℃;

DOI:10.1023/B:RUGC.0000016014.90042.3b

upstream raw materials:

1,2-O-isopropylideneglycero-3-(benzyldiethylphosphoramidite)

N-Methyldiethanolamine

Downstream raw materials:

phosphoric acid benzyl ester 2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-methyl-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

thiophosphoric acid O-benzyl ester O'-[2-({2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-thiophosphoryloxy]-ethyl}-methyl-amino)-ethyl] ester O''-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl) ester

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