N-(4-(2,3-dichloro-4-nitrophenoxy)pyridin-2-yl)-2-morpholino acetamide

Base Information

Chemical Name:N-(4-(2,3-dichloro-4-nitrophenoxy)pyridin-2-yl)-2-morpholino acetamide
CAS No.:1337931-88-0
Molecular Formula:C₁₇H₁₆Cl₂N₄O₅
Molecular Weight:427.244
Hs Code.:

Synonyms:N-(4-(2,3-dichloro-4-nitrophenoxy)pyridin-2-yl)-2-morpholino acetamide

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Chemical Property of N-(4-(2,3-dichloro-4-nitrophenoxy)pyridin-2-yl)-2-morpholino acetamide

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Technology Process of N-(4-(2,3-dichloro-4-nitrophenoxy)pyridin-2-yl)-2-morpholino acetamide

There total 3 articles about N-(4-(2,3-dichloro-4-nitrophenoxy)pyridin-2-yl)-2-morpholino acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 1337931-94-8
4-(2,3-dichloro-4-nitrophenoxy)pyridin-2-amine

: 79-04-9
chloroacetyl chloride

: 1337931-88-0
N-(4-(2,3-dichloro-4-nitrophenoxy)pyridin-2-yl)-2-morpholino acetamide

Guidance literature:: 4-(2,3-dichloro-4-nitrophenoxy)pyridin-2-amine; chloroacetyl chloride; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; for 4h; Inert atmosphere;

morpholine; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; for 16h; Inert atmosphere;

With sodium hydrogencarbonate; In tetrahydrofuran; water;

Reference yield:

: 33631-05-9
2-amino-4-hydroxypyridine

: 1337931-88-0
N-(4-(2,3-dichloro-4-nitrophenoxy)pyridin-2-yl)-2-morpholino acetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.5 h / 20 °C

1.2: 16 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

2.2: 16 h / 0 - 20 °C / Inert atmosphere

With 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile;

Reference yield:

: 36556-51-1
2,3-dichloro-1-fluoro-4-nitrobenzene

: 1337931-88-0
N-(4-(2,3-dichloro-4-nitrophenoxy)pyridin-2-yl)-2-morpholino acetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.5 h / 20 °C

1.2: 16 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

2.2: 16 h / 0 - 20 °C / Inert atmosphere

With 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile;