5′-O-(4,4′-dimethoxytriphenylmethyl)-2′-O-azidoprop-1-yl-6-N-benzoyladenosine

Base Information

• Chemical Name: 5′-O-(4,4′-dimethoxytriphenylmethyl)-2′-O-azidoprop-1-yl-6-N-benzoyladenosine
• CAS No.: 1005190-89-5
• Molecular Formula: C₄₁H₄₀N₈O₇
• Molecular Weight: 756.818

Synonyms:5′-O-(4,4′-dimethoxytriphenylmethyl)-2′-O-azidoprop-1-yl-6-N-benzoyladenosine

Chemical Property of 5′-O-(4,4′-dimethoxytriphenylmethyl)-2′-O-azidoprop-1-yl-6-N-benzoyladenosine

Chemical Property:

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Technology Process of 5′-O-(4,4′-dimethoxytriphenylmethyl)-2′-O-azidoprop-1-yl-6-N-benzoyladenosine

There total 1 articles about 5′-O-(4,4′-dimethoxytriphenylmethyl)-2′-O-azidoprop-1-yl-6-N-benzoyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2'-O-(3-azidoprop-1-yl)-6-N-benzoyladenosine (1005190-69-1) + 4,4'-dimethoxytrityl chloride (40615-36-9) → 5′-O-(4,4′-dimethoxytriphenylmethyl)-2′-O-azidoprop-1-yl-6-N-benzoyladenosine (1005190-89-5)

Guidance literature:

With pyridine; at 20 ℃; for 3h;

DOI:10.1021/jo702023s

Reference yield: 19.0%

5′-O-(4,4′-dimethoxytriphenylmethyl)-2′-O-azidoprop-1-yl-6-N-benzoyladenosine (1005190-89-5) + 2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) → 5'-O-(di(4-methoxyphenyl)(phenyl)methyl)-2'-O-(3-azidoprop-1-yl)-6-N-benzoyladenosine-3'-O-(2-cyanoethyl N,N-diisopropylphosphoramidite) (1005190-71-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 1h;

DOI:10.1021/jo702023s

Reference yield:

5′-O-(4,4′-dimethoxytriphenylmethyl)-2′-O-azidoprop-1-yl-6-N-benzoyladenosine (1005190-89-5) → C41H42N6O7

Guidance literature:

With trimethylphosphane; In tetrahydrofuran; water; at 20 ℃; for 8h; Inert atmosphere;

DOI:10.3390/molecules18077346

upstream raw materials:

2'-O-(3-azidoprop-1-yl)-6-N-benzoyladenosine

4,4'-dimethoxytrityl chloride

Downstream raw materials:

5'-O-(di(4-methoxyphenyl)(phenyl)methyl)-2'-O-(3-azidoprop-1-yl)-6-N-benzoyladenosine-3'-O-(2-cyanoethyl N,N-diisopropylphosphoramidite)

5′-O-(4,4′-dimethoxytriphenylmethyl)-2′-O-(9H-fluoren-9-yl-methylcarbonyl)aminoprop-1-yl-6-Nbenzoyladenosine-3′-O-(2-cyanoethyl N,N-diisopropylphosphoramidite)

5′-O-(4,4′-dimethoxytriphenylmethyl)-2′-O-(9H-fluoren-9-yl-methylcarbonyl)-aminoprop-1-yl-6-N-benzoyladenosine

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