[(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methylether)Cu(CO)]PF₆

Base Information

• Chemical Name: [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methylether)Cu(CO)]PF₆
• CAS No.: 932712-42-0
• Molecular Formula: CO*C₅₀H₄₂N₆O*Cu*F₆P
• Molecular Weight: 979.444

Synonyms:[(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methylether)Cu(CO)]PF₆

Chemical Property of [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methylether)Cu(CO)]PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Technology Process of [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methylether)Cu(CO)]PF₆

There total 3 articles about [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methylether)Cu(CO)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol (189071-85-0) + tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methyl ether (932711-97-2) + carbon monoxide (201230-82-2) → [(6,9-dimesityl-2-(4-bromophenyl)imidazo[4,5-f]-1,10-phenanthroline)Cu(2,9-dimethyl-1,10-phenanthroline)][P(fluoride)6]*methanol + [(3,6-di-n-butyl-11-bromodipyrido[2,3-c:3',2'-a]phenazine)Cu(6,9-dimesityl-2-(4-bromophenyl)imidazo[4,5-f]-1,10-phenanthroline)][P(fluoride)6]*2(methanol) + [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol)Cu(CO)]PF6 (932712-36-2) + [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methylether)Cu(CO)]PF6 (932712-42-0) + [(6,9-dimesityl-2-(4-bromophenyl)imidazo[4,5-f]-1,10-phenanthroline)Cu(1,10-phenanthroline)][P(fluoride)6]*(methanol) + [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol)Cu]2(PF6)2 + [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methylether)Cu]2(PF6)2

Guidance literature:

In acetonitrile; for 2h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1039/c6dt04390a

Reference yield:

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol (189071-85-0) + tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methyl ether (932711-97-2) + carbon monoxide (201230-82-2) → [(6,9-dimesityl-2-(4-bromophenyl)imidazo[4,5-f]-1,10-phenanthroline)Cu(2,9-dimethyl-1,10-phenanthroline)][P(fluoride)6]*methanol + [(3,6-di-n-butyl-11-bromodipyrido[2,3-c:3',2'-a]phenazine)Cu(6,9-dimesityl-2-(4-bromophenyl)imidazo[4,5-f]-1,10-phenanthroline)][P(fluoride)6]*2(methanol) + [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol)Cu(CO)]PF6 (932712-36-2) + [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methylether)Cu(CO)]PF6 (932712-42-0) + [(6,9-dimesityl-2-(4-bromophenyl)imidazo[4,5-f]-1,10-phenanthroline)Cu(1,10-phenanthroline)][P(fluoride)6]*(methanol)

Guidance literature:

In dichloromethane; Schlenk techniques, under N2; Cu complex stirred in CH2Cl2, soln. of (NC5H4CHN)2(C2H4) (1 equiv.) added, stirred at room temp. for 12 h; solvent removed under vac.; elem. anal.;

DOI:10.1002/ejic.201101414

Reference yield:

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol (189071-85-0) + tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methyl ether (932711-97-2) + carbon monoxide (201230-82-2) → [(6,9-dimesityl-2-(4-bromophenyl)imidazo[4,5-f]-1,10-phenanthroline)Cu(2,9-dimethyl-1,10-phenanthroline)][P(fluoride)6]*methanol + [(3,6-di-n-butyl-11-bromodipyrido[2,3-c:3',2'-a]phenazine)Cu(6,9-dimesityl-2-(4-bromophenyl)imidazo[4,5-f]-1,10-phenanthroline)][P(fluoride)6]*2(methanol) + [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol)Cu(CO)]PF6 (932712-36-2) + [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methylether)Cu(CO)]PF6 (932712-42-0) + [(6,9-dimesityl-2-(4-bromophenyl)imidazo[4,5-f]-1,10-phenanthroline)Cu(1,10-phenanthroline)][P(fluoride)6]*(methanol) + [(tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol)Cu]2(PF6)2

Guidance literature:

In dichloromethane; Schlenk techniques, under N2; Cu complex stirred in CH2Cl2, soln. of (NC5H4CHN)2(C2H4) (1 equiv.) added, stirred at room temp. for 12 h; solvent removed under vac.; elem. anal.;

DOI:10.1002/ejic.201101414

upstream raw materials:

tetrakis(actonitrile)copper(I) hexafluorophosphate

tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol

tris(1-methyl-4,5-diphenylimidazol-2-yl)methanol methyl ether

carbon monoxide

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