[3,12-dihydroxy-6,9-dimethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]trimethylsilane

Base Information

Chemical Name:[3,12-dihydroxy-6,9-dimethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]trimethylsilane
CAS No.:1421518-46-8
Molecular Formula:C₄₆H₄₆O₄Si₂
Molecular Weight:719.04
Hs Code.:

Synonyms:[3,12-dihydroxy-6,9-dimethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]trimethylsilane

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Chemical Property of [3,12-dihydroxy-6,9-dimethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]trimethylsilane

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Technology Process of [3,12-dihydroxy-6,9-dimethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]trimethylsilane

There total 1 articles about [3,12-dihydroxy-6,9-dimethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]trimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 13829-77-1
3-(trimethylsilyl)-1-phenyl-2-propyn-1-one

: 801287-69-4
3,6-dimethoxy-3,6-diphenylocta-1,4,7-triyne

: 1421518-46-8
[3,12-dihydroxy-6,9-dimethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]trimethylsilane

Guidance literature:: 3,6-dimethoxy-3,6-diphenylocta-1,4,7-triyne; With ethylmagnesium bromide; In tetrahydrofuran; at 0 - 20 ℃; for 1.25h; Inert atmosphere; Schlenk technique;

3-(trimethylsilyl)-1-phenyl-2-propyn-1-one; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201201555

Reference yield: 100.0%

: 1421518-46-8
[3,12-dihydroxy-6,9-dimethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]trimethylsilane

: 74-88-4
methyl iodide

: 945392-92-7
trimethyl[3,6,9,12-tetramethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]silane

Guidance literature:: [3,12-dihydroxy-6,9-dimethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]trimethylsilane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.25h; Inert atmosphere; Schlenk technique;

methyl iodide; In tetrahydrofuran; at -78 - -30 ℃; Inert atmosphere; Schlenk technique;

With dimethyl sulfoxide; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201201555