trimethyl[3,6,9,12-tetramethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]silane

Base Information

Chemical Name:trimethyl[3,6,9,12-tetramethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]silane
CAS No.:945392-92-7
Molecular Formula:C₄₈H₅₀O₄Si₂
Molecular Weight:747.094
Hs Code.:

Synonyms:trimethyl[3,6,9,12-tetramethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]silane

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Chemical Property of trimethyl[3,6,9,12-tetramethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]silane

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Technology Process of trimethyl[3,6,9,12-tetramethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]silane

There total 2 articles about trimethyl[3,6,9,12-tetramethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1421518-46-8
[3,12-dihydroxy-6,9-dimethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]trimethylsilane

: 74-88-4
methyl iodide

: 945392-92-7
trimethyl[3,6,9,12-tetramethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]silane

Guidance literature:: [3,12-dihydroxy-6,9-dimethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]trimethylsilane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.25h; Inert atmosphere; Schlenk technique;

methyl iodide; In tetrahydrofuran; at -78 - -30 ℃; Inert atmosphere; Schlenk technique;

With dimethyl sulfoxide; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201201555

Reference yield: 95.0%

: 945392-91-6
1,14-bis(trimethylsilyl)-3,12-dimethoxy-3,6,9,12-tetraphenyltetradeca-1,4,7,10,13-pentayne-6,9-diol

: 74-88-4
methyl iodide

: 945392-92-7
trimethyl[3,6,9,12-tetramethoxy-3,6,9,12-tetraphenyl-14-(trimethylsilyl)tetradeca-1,4,7,10,13-pentayn-1-yl]silane

Guidance literature:: 1,14-bis(trimethylsilyl)-3,12-dimethoxy-3,6,9,12-tetraphenyltetradeca-1,4,7,10,13-pentayne-6,9-diol; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h;

methyl iodide; In tetrahydrofuran; hexane; dimethyl sulfoxide; at -25 - 20 ℃; for 4h; Further stages.;
DOI:10.1002/chem.200601191