N₁,N₃-bis(2-(4-hydroxyphenoxy)ethyl)-5-ferrocenylisophthalamide

Base Information

• Chemical Name: N₁,N₃-bis(2-(4-hydroxyphenoxy)ethyl)-5-ferrocenylisophthalamide
• CAS No.: 1262899-08-0
• Molecular Formula: C₃₄H₃₂FeN₂O₆
• Molecular Weight: 620.485
• Mol file: 1262899-08-0.mol

Synonyms:N₁,N₃-bis(2-(4-hydroxyphenoxy)ethyl)-5-ferrocenylisophthalamide

Chemical Property of N₁,N₃-bis(2-(4-hydroxyphenoxy)ethyl)-5-ferrocenylisophthalamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N₁,N₃-bis(2-(4-hydroxyphenoxy)ethyl)-5-ferrocenylisophthalamide

There total 1 articles about N₁,N₃-bis(2-(4-hydroxyphenoxy)ethyl)-5-ferrocenylisophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N1,N3-bis(2-(4-(benzyloxy)phenoxy)ethyl)-5-ferrocenylisophthalamide (1262899-07-9) + hydrogen (1333-74-0) → N1,N3-bis(2-(4-hydroxyphenoxy)ethyl)-5-ferrocenylisophthalamide (1262899-08-0)

Guidance literature:

With Pd/C; In methanol; chloroform; Pd/C added to a soln. of Fe complex in CHCl3/MeOH, stirred under H2 for 16 h; filtered, evapd. (vac.);

DOI:10.1039/c0ob00458h

Reference yield: 48.0%

N1,N3-bis(2-(4-hydroxyphenoxy)ethyl)-5-ferrocenylisophthalamide (1262899-08-0) + 2-(allyloxy)ethyl 4-methylbenzenesulfonate (50563-72-9) → N1,N3-bis(2-(4-(2-(allyloxy)ethoxy)phenoxy)ethyl)-5-ferrocenylisophthalamide (1262899-05-7)

Guidance literature:

With K₂CO₃; In acetonitrile; Fe complex, CH2CHCH2OC2H4OSO2C6H4CH3 and K2CO3 suspended in MeCN, heatedunder N2 for 60 h; cooled to room temp., filtered, evapd. (vac.), dissolved in CH2Cl2, filtered, dried (MgSO4), evapd. (vac.), chromd. (silica gel, CH2Cl2/MeOH); obtained as oil;

DOI:10.1039/c0ob00458h

upstream raw materials:

N₁,N₃-bis(2-(4-(benzyloxy)phenoxy)ethyl)-5-ferrocenylisophthalamide

hydrogen

Downstream raw materials:

N₁,N₃-bis(2-(4-(2-(allyloxy)ethoxy)phenoxy)ethyl)-5-ferrocenylisophthalamide