1-Iodoethyl ethyl carbonate

Base Information

• Chemical Name: 1-Iodoethyl ethyl carbonate
• CAS No.: 80196-04-9
• Molecular Formula: C5H9IO3
• Molecular Weight: 244.03
• DSSTox Substance ID: DTXSID60438961
• Nikkaji Number: J675.339F
• Mol file: 80196-04-9.mol

Synonyms:1-IODOETHYL ETHYL CARBONATE;80196-04-9;Ethyl 1-iodoethyl Carbonate;1-Iodoethylethylcarbonate;SCHEMBL304485;1-(ethoxycarbonyloxy)ethyl iodide;DTXSID60438961;BDHXJIRTSWHBPR-UHFFFAOYSA-N;AKOS015963371;Carbonic acid ethyl(1-iodoethyl) ester;CS-0498527

Chemical Property of 1-Iodoethyl ethyl carbonate

Chemical Property:

• Vapor Pressure: 0.542mmHg at 25°C
• Refractive Index: 1.506
• Boiling Point: 190.4 °C at 760 mmHg
• Flash Point: 69 °C
• PSA: 35.53000
• Density: 1.741 g/cm³
• LogP: 1.94050
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 243.95964
• Heavy Atom Count: 9
• Complexity: 94.2

Purity/Quality:

99% ^*data from raw suppliers

1-IODOETHYL ETHYL CARBONATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(=O)OC(C)I

Technology Process of 1-Iodoethyl ethyl carbonate

There total 3 articles about 1-Iodoethyl ethyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

1-Chloroethyl ethyl carbonate (50893-36-2) → ethyl 1-iodoethylcarbonate (80196-04-9)

Guidance literature:

With sodium iodide; In acetonitrile; at 60 ℃; for 6h;

Reference yield: 10.0%

1-Chloroethyl ethyl carbonate (50893-36-2) → 7β-(2-cyano-n-butyryl)amino-7α-methoxy-3-(1-methyl-5-tetrazolyl)thiomethyl-1-dethia-1-oxa-3-cephem-4 -carboxylic acid 1-(ethoxycarbonyloxy)ethyl ester + ethyl 1-iodoethylcarbonate (80196-04-9)

Guidance literature:

With sodium iodide; In water; acetone;

Reference yield:

→ ethyl 1-iodoethylcarbonate (80196-04-9)

Guidance literature:

upstream raw materials:

1-Chloroethyl ethyl carbonate

Downstream raw materials:

(4R,5S,6S)-6-((R)-1-Hydroxy-ethyl)-4-methyl-3-{(2R,3R)-2-[(4-nitro-benzyloxycarbonylamino)-methyl]-tetrahydro-furan-3-ylsulfanyl}-7-oxo-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 1-ethoxycarbonyloxy-ethyl ester

1-ethoxycarbonyloxyethyl 2,7-diethyl-5-[[2'-(N-triphenylmethyl-tetrazol-5-yl)biphenyl-4-yl]methyl]-5H-pyrazolo[1,5-b][1,2,4]triazole-6-carboxylate

2-Butyl-5-[methyl-(3-methyl-but-2-enoyl)-amino]-3-[2'-(1-trityl-1H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-3H-imidazole-4-carboxylic acid 1-ethoxycarbonyloxy-ethyl ester

1-(ethoxycarbonyloxy)ethyl (6R,7R)-7-[(Z)-2-(2-amino-4-thiazolyl)-2-(methoxyimino)acetamido]-3-(methoxymethyl)-3-cephem-4-carboxylate