1,2-bis[5'-((1S)-1,2,2-trimethylcyclopentyl)-3',4'-dimethoxyphenyl]ethane

Base Information

Chemical Name:1,2-bis[5'-((1S)-1,2,2-trimethylcyclopentyl)-3',4'-dimethoxyphenyl]ethane
CAS No.:333401-68-6
Molecular Formula:C₃₄H₅₀O₄
Molecular Weight:522.769
Hs Code.:

Synonyms:1,2-bis[5'-((1S)-1,2,2-trimethylcyclopentyl)-3',4'-dimethoxyphenyl]ethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bis[5'-((1S)-1,2,2-trimethylcyclopentyl)-3',4'-dimethoxyphenyl]ethane

Chemical Property:

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Technology Process of 1,2-bis[5'-((1S)-1,2,2-trimethylcyclopentyl)-3',4'-dimethoxyphenyl]ethane

There total 5 articles about 1,2-bis[5'-((1S)-1,2,2-trimethylcyclopentyl)-3',4'-dimethoxyphenyl]ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₄H₄₈O₄

: 333401-68-6
1,2-bis[5'-((1S)-1,2,2-trimethylcyclopentyl)-3',4'-dimethoxyphenyl]ethane

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate; under 760 Torr;
DOI:10.1016/S0040-4020(00)01131-5

Reference yield:

: (S)-5-bromomethyl-1,2-dimethoxy-3-(1,2,2-trimethylcyclopentyl)benzene

: 333401-68-6
1,2-bis[5'-((1S)-1,2,2-trimethylcyclopentyl)-3',4'-dimethoxyphenyl]ethane

Guidance literature:: Multi-step reaction with 4 steps

1: CaCO₃; water / dioxane / Heating

2: 230 mg / MnO₂ / CH₂Cl₂ / 40 °C / ultrasonic irradiation

3: zinc; TiCl₄ / tetrahydrofuran / 2 h / Heating

4: 63.0 mg / H₂ / Pd/C / ethanol; ethyl acetate / 760 Torr

With manganese(IV) oxide; water; hydrogen; titanium tetrachloride; calcium carbonate; zinc; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(00)01131-5

Reference yield:

: 222022-92-6
(1'S)-3,4-dimethoxy-5-(1',2',2'-trimethylcyclopentyl)benzyl alcohol

: 333401-68-6
1,2-bis[5'-((1S)-1,2,2-trimethylcyclopentyl)-3',4'-dimethoxyphenyl]ethane

Guidance literature:: Multi-step reaction with 3 steps

1: 230 mg / MnO₂ / CH₂Cl₂ / 40 °C / ultrasonic irradiation

2: zinc; TiCl₄ / tetrahydrofuran / 2 h / Heating

3: 63.0 mg / H₂ / Pd/C / ethanol; ethyl acetate / 760 Torr

With manganese(IV) oxide; hydrogen; titanium tetrachloride; zinc; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(00)01131-5