N,N-dibenzyl-2-oxo-2-phenyl-thioacetamide

Base Information

Chemical Name:N,N-dibenzyl-2-oxo-2-phenyl-thioacetamide
CAS No.:623943-06-6
Molecular Formula:C₂₂H₁₉NOS
Molecular Weight:345.465
Hs Code.:

<i>N</i>,<i>N</i>-dibenzyl-2-oxo-2-phenyl-thioacetamide

Synonyms:N,N-dibenzyl-2-oxo-2-phenyl-thioacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-dibenzyl-2-oxo-2-phenyl-thioacetamide

Chemical Property:

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Technology Process of N,N-dibenzyl-2-oxo-2-phenyl-thioacetamide

There total 1 articles about N,N-dibenzyl-2-oxo-2-phenyl-thioacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 98-86-2
acetophenone

: 103-49-1
dibenzylamine

: 623943-06-6
N,N-dibenzyl-2-oxo-2-phenyl-thioacetamide

Guidance literature:: acetophenone; With pyridine; thionyl chloride; at 20 ℃; for 48h;

dibenzylamine; With sodium hydroxide; In chloroform; at 20 ℃; for 2h;
DOI:10.1080/00304940209355761

Reference yield: 50.0%

: 623943-06-6
N,N-dibenzyl-2-oxo-2-phenyl-thioacetamide

: 501012-83-5
N,N-dibenzyl-2-phenyl-2-thioxo-thioacetamide

Guidance literature:: With Lawessons reagent; In toluene; for 10h; Heating;
DOI:10.1080/00304940209355761

Reference yield:

: 623943-06-6
N,N-dibenzyl-2-oxo-2-phenyl-thioacetamide

: 4-dibenzylamino-2,5-diphenyl-[1,3]dithiole-2-carbothioic acid dibenzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / Lawesson reagent / toluene / 10 h / Heating

2: 56 percent / trimethyl phosphite / diethyl ether / 10 h / 20 °C

With Lawessons reagent; phosphorous acid trimethyl ester; In diethyl ether; toluene;
DOI:10.1080/00304940209355761