(2E,4E,6E)-8-<4-(4-bromobenzyloxy)-1,2-dihydro-1-methyl-2-oxo-3-pyridinyl>-7-methyl-8-oxo-2,4,6-octatrienoic acid

Base Information

Chemical Name:(2E,4E,6E)-8-<4-(4-bromobenzyloxy)-1,2-dihydro-1-methyl-2-oxo-3-pyridinyl>-7-methyl-8-oxo-2,4,6-octatrienoic acid
CAS No.:51067-69-7
Molecular Formula:C₂₂H₂₀BrNO₅
Molecular Weight:458.308
Hs Code.:

Synonyms:(2E,4E,6E)-8-<4-(4-bromobenzyloxy)-1,2-dihydro-1-methyl-2-oxo-3-pyridinyl>-7-methyl-8-oxo-2,4,6-octatrienoic acid

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Chemical Property of (2E,4E,6E)-8-<4-(4-bromobenzyloxy)-1,2-dihydro-1-methyl-2-oxo-3-pyridinyl>-7-methyl-8-oxo-2,4,6-octatrienoic acid

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Technology Process of (2E,4E,6E)-8-<4-(4-bromobenzyloxy)-1,2-dihydro-1-methyl-2-oxo-3-pyridinyl>-7-methyl-8-oxo-2,4,6-octatrienoic acid

There total 5 articles about (2E,4E,6E)-8-<4-(4-bromobenzyloxy)-1,2-dihydro-1-methyl-2-oxo-3-pyridinyl>-7-methyl-8-oxo-2,4,6-octatrienoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51067-68-6
goldinamine(4-bromobenzyl) ether

: 64-18-6
formic acid

: 51067-69-7
(2E,4E,6E)-8-<4-(4-bromobenzyloxy)-1,2-dihydro-1-methyl-2-oxo-3-pyridinyl>-7-methyl-8-oxo-2,4,6-octatrienoic acid

: 51067-70-0,53152-54-8
(4E,6E)-8-Amino-3-methoxy-2,4-dimethyl-octa-4,6-dienal

Guidance literature:: With barium dihydroxide; sodium hydroxide; sodium periodate; sulfuric acid; acetic anhydride;
DOI:10.1139/v80-080

Reference yield:

: aurodox

: 51067-69-7
(2E,4E,6E)-8-<4-(4-bromobenzyloxy)-1,2-dihydro-1-methyl-2-oxo-3-pyridinyl>-7-methyl-8-oxo-2,4,6-octatrienoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide / 72 h / Ambient temperature

2: acetic acid / 72 h / Ambient temperature

3: sodium metaperiodate

With sodium periodate; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1139/v80-080

Reference yield:

: 589-15-1
1-bromomethyl-4-bromobenzene

: 51067-69-7
(2E,4E,6E)-8-<4-(4-bromobenzyloxy)-1,2-dihydro-1-methyl-2-oxo-3-pyridinyl>-7-methyl-8-oxo-2,4,6-octatrienoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide / 72 h / Ambient temperature

2: acetic acid / 72 h / Ambient temperature

3: sodium metaperiodate

With sodium periodate; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1139/v80-080