[(tetrahydrofuran)₂Li{(2,6-diisopropylphenylamine)C(tert-butyl)NCH₂-2-furanyl}]

Base Information

Chemical Name:[(tetrahydrofuran)₂Li{(2,6-diisopropylphenylamine)C(tert-butyl)NCH₂-2-furanyl}]
CAS No.:1574503-15-3
Molecular Formula:C₃₀H₄₇LiN₂O₃
Molecular Weight:490.656
Hs Code.:

[(tetrahydrofuran)<sub>2</sub>Li{(2,6-diisopropylphenylamine)C(tert-butyl)NCH<sub>2</sub>-2-furanyl}]

Synonyms:[(tetrahydrofuran)₂Li{(2,6-diisopropylphenylamine)C(tert-butyl)NCH₂-2-furanyl}]

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Chemical Property of [(tetrahydrofuran)₂Li{(2,6-diisopropylphenylamine)C(tert-butyl)NCH₂-2-furanyl}]

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Technology Process of [(tetrahydrofuran)₂Li{(2,6-diisopropylphenylamine)C(tert-butyl)NCH₂-2-furanyl}]

There total 5 articles about [(tetrahydrofuran)₂Li{(2,6-diisopropylphenylamine)C(tert-butyl)NCH₂-2-furanyl}] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 1574622-42-6
1-(2-furanylmethyl)-2-tert-butyl-3-(2,6-diisopropylphenyl)-1,3-diazaprop-2-ene

: 1574503-15-3
[(tetrahydrofuran)₂Li{(2,6-diisopropylphenylamine)C(tert-butyl)NCH₂-2-furanyl}]

Guidance literature:: 1-(2-furanylmethyl)-2-tert-butyl-3-(2,6-diisopropylphenyl)-1,3-diazaprop-2-ene; With n-butyllithium; In hexane; pentane; at -78 - 20 ℃; for 4h; Inert atmosphere; Schlenk technique;

tetrahydrofuran; at -20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/om500135g

Reference yield:

: 215715-81-4
N-(2,6-diisopropylphenyl)tert-butyl amide

: 1574503-15-3
[(tetrahydrofuran)₂Li{(2,6-diisopropylphenylamine)C(tert-butyl)NCH₂-2-furanyl}]

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / Inert atmosphere; Schlenk technique

2.1: Inert atmosphere; Schlenk technique

3.1: n-butyllithium / hexane; pentane / 4 h / -78 - 20 °C / Inert atmosphere; Schlenk technique

3.2: -20 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; thionyl chloride; In hexane; pentane;
DOI:10.1021/om500135g

Reference yield:

: N-(2,6-diisopropylphenyl)-2,2-dimethylpropionimidoyl chloride

: 1574503-15-3
[(tetrahydrofuran)₂Li{(2,6-diisopropylphenylamine)C(tert-butyl)NCH₂-2-furanyl}]

Guidance literature:: Multi-step reaction with 2 steps

1.1: Inert atmosphere; Schlenk technique

2.1: n-butyllithium / hexane; pentane / 4 h / -78 - 20 °C / Inert atmosphere; Schlenk technique

2.2: -20 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; In hexane; pentane;
DOI:10.1021/om500135g