1-(2-furanylmethyl)-2-tert-butyl-3-(2,6-diisopropylphenyl)-1,3-diazaprop-2-ene

Base Information

• Chemical Name: 1-(2-furanylmethyl)-2-tert-butyl-3-(2,6-diisopropylphenyl)-1,3-diazaprop-2-ene
• CAS No.: 1574622-42-6
• Molecular Formula: C₂₂H₃₂N₂O
• Molecular Weight: 340.509

Synonyms:1-(2-furanylmethyl)-2-tert-butyl-3-(2,6-diisopropylphenyl)-1,3-diazaprop-2-ene

Chemical Property of 1-(2-furanylmethyl)-2-tert-butyl-3-(2,6-diisopropylphenyl)-1,3-diazaprop-2-ene

Chemical Property:

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Technology Process of 1-(2-furanylmethyl)-2-tert-butyl-3-(2,6-diisopropylphenyl)-1,3-diazaprop-2-ene

There total 4 articles about 1-(2-furanylmethyl)-2-tert-butyl-3-(2,6-diisopropylphenyl)-1,3-diazaprop-2-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

furan-2-ylmethanamine (617-89-0) + N-(2,6-diisopropylphenyl)-2,2-dimethylpropionimidoyl chloride → 1-(2-furanylmethyl)-2-tert-butyl-3-(2,6-diisopropylphenyl)-1,3-diazaprop-2-ene (1574622-42-6)

Guidance literature:

Inert atmosphere; Schlenk technique;

DOI:10.1021/om500135g

Reference yield:

2,6-diisopropylbenzenamine (24544-04-5) → 1-(2-furanylmethyl)-2-tert-butyl-3-(2,6-diisopropylphenyl)-1,3-diazaprop-2-ene (1574622-42-6)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / Inert atmosphere; Schlenk technique

2: thionyl chloride / Inert atmosphere; Schlenk technique

3: Inert atmosphere; Schlenk technique

With pyridine; thionyl chloride;

DOI:10.1021/om500135g

Reference yield:

pivaloyl chloride (3282-30-2) → 1-(2-furanylmethyl)-2-tert-butyl-3-(2,6-diisopropylphenyl)-1,3-diazaprop-2-ene (1574622-42-6)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / Inert atmosphere; Schlenk technique

2: thionyl chloride / Inert atmosphere; Schlenk technique

3: Inert atmosphere; Schlenk technique

With pyridine; thionyl chloride;

DOI:10.1021/om500135g

upstream raw materials:

2,6-diisopropylbenzenamine

pivaloyl chloride

N-(2,6-diisopropylphenyl)tert-butyl amide

furan-2-ylmethanamine

Downstream raw materials:

[(tetrahydrofuran)₂Li{(2,6-diisopropylphenylamine)C(tert-butyl)NCH₂-2-furanyl}]

bis[1-(2-furanylmethyl)-2-tertbutyl-3-(2,6-diisopropylphenyl)-1,3-diazaallyl]calcium

[(1,2-dimethoxyethane)K{(2,6-diisopropylphenylamine)C(tert-butyl)CH₂-2-furanyl}]

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