(-)-(βR,2S)-β-Phenylspirodithiolan>-2-propansaeure-methylester

Base Information

Chemical Name:(-)-(βR,2S)-β-Phenylspirodithiolan>-2-propansaeure-methylester
CAS No.:86661-28-1
Molecular Formula:C₁₈H₂₄O₂S₂
Molecular Weight:336.519
Hs Code.:

(-)-(βR,2S)-β-Phenylspiro<cyclohexan-1,2'-<1,3>dithiolan>-2-propansaeure-methylester

Synonyms:(-)-(βR,2S)-β-Phenylspirodithiolan>-2-propansaeure-methylester

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Chemical Property of (-)-(βR,2S)-β-Phenylspirodithiolan>-2-propansaeure-methylester

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Technology Process of (-)-(βR,2S)-β-Phenylspirodithiolan>-2-propansaeure-methylester

There total 3 articles about (-)-(βR,2S)-β-Phenylspirodithiolan>-2-propansaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 540-63-6
ethane-1,2-dithiol

: 86661-27-0
(-)-(3R,1'S)-3-(2-Oxocyclohexyl)-3-phenylpropansaeure-methylester

: 86661-28-1
(-)-(βR,2S)-β-Phenylspirodithiolan>-2-propansaeure-methylester

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃;

Reference yield:

: 6626-84-2
dimethyl 2-benzylidenepropanedioate

: 86661-28-1
(-)-(βR,2S)-β-Phenylspirodithiolan>-2-propansaeure-methylester

Guidance literature:: Multi-step reaction with 3 steps

1: 2) 2 N HCl, H₂O / 1) ether, 7 d, r.t., 2) CH₂Cl₂, 80 deg C

2: 58 percent / KOH / methanol / Ambient temperature

3: 45 percent / BF₃*Et₂O / CH₂Cl₂ / 0 °C

With hydrogenchloride; potassium hydroxide; boron trifluoride diethyl etherate; water; In methanol; dichloromethane;

Reference yield:

: 86661-23-6
dimethyl 2‐{(S)‐phenyl[(1S)‐2‐oxocyclohexyl]methyl}propanedioate

: 86661-28-1
(-)-(βR,2S)-β-Phenylspirodithiolan>-2-propansaeure-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / KOH / methanol / Ambient temperature

2: 45 percent / BF₃*Et₂O / CH₂Cl₂ / 0 °C

With potassium hydroxide; boron trifluoride diethyl etherate; In methanol; dichloromethane;