(3S,4R)-3,4-dimethylcyclohexanone

Base Information

Chemical Name:(3S,4R)-3,4-dimethylcyclohexanone
CAS No.:75364-88-4
Molecular Formula:C₈H₁₄O
Molecular Weight:126.199
Hs Code.:

Synonyms:(3S,4R)-3,4-dimethylcyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4R)-3,4-dimethylcyclohexanone

Chemical Property:

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Technology Process of (3S,4R)-3,4-dimethylcyclohexanone

There total 18 articles about (3S,4R)-3,4-dimethylcyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 6876-23-9
1,2-trans-dimethylcyclohexane

: 19879-11-9
1,2-dimethylcyclohexanol

: 1551-89-9
trans-2,3-dimethylcyclohexanone

: 5465-09-8,27922-05-0,28023-45-2,69127-34-0,75364-86-2,75364-88-4,75364-89-5,113348-79-1
trans-1,2-dimethyl-cyclohexan-4-one

Guidance literature:: With methyltrifluoromethyldioxirane; In dichloromethane; at -22 ℃; for 0.166667h; Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja00199a039

Reference yield: 75.0%

: 75337-05-2,79980-78-2,101758-35-4,5515-76-4
4-methyl-2-cyclohexenone

: 917-54-4
methyllithium

: 5465-09-8,27922-05-0,28023-45-2,69127-34-0,75364-86-2,75364-88-4,75364-89-5,113348-79-1
trans-1,2-dimethyl-cyclohexan-4-one

Guidance literature:: methyllithium; With copper(l) cyanide; In diethyl ether; at -78 - 0 ℃; Inert atmosphere;

4-methyl-2-cyclohexenone; In diethyl ether; at -78 ℃; Inert atmosphere;

With water; ammonium chloride; In diethyl ether; Inert atmosphere;
DOI:10.1002/anie.201304359

Reference yield: 10.0%

: 2207-01-4
cis-1,2-dimethylcyclohexane

: 1174149-28-0
cis-1,2-dimethylcyclohexan-1-ol

: 385423-97-2
(2S,3S)-2,3-dimethylcyclohexanone

: 1174149-18-8
trans-1,2-dimethylcyclohexan-1-ol

: 75364-88-4
(3S,4R)-3,4-dimethylcyclohexanone

Guidance literature:: With C₃₃H₂₈FeN₆⁽²⁺⁾*2ClO₄^(1-); 2-iodylbenzoic acid 1-methylethyl ester; In acetonitrile; for 3h; Catalytic behavior;
DOI:10.1039/d1dt03381f