(2S,3S)-2,3-Dimethylcyclohexanone

Base Information

Chemical Name:(2S,3S)-2,3-Dimethylcyclohexanone
CAS No.:385423-97-2
Molecular Formula:C₈H₁₄O
Molecular Weight:126.199
Hs Code.:
DSSTox Substance ID:DTXSID301298702
Nikkaji Number:J523.049G

Synonyms:SCHEMBL16554317;DTXSID301298702;(2S,3S)-2,3-Dimethylcyclohexanone;385423-97-2

Suppliers and Price of (2S,3S)-2,3-Dimethylcyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-2,3-Dimethylcyclohexanone

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:126.104465066
Heavy Atom Count:9
Complexity:118

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1CCCC(=O)C1C
Isomeric SMILES:C[C@H]1CCCC(=O)[C@H]1C

Technology Process of (2S,3S)-2,3-Dimethylcyclohexanone

There total 10 articles about (2S,3S)-2,3-Dimethylcyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 2207-01-4
cis-1,2-dimethylcyclohexane

: 1174149-28-0
cis-1,2-dimethylcyclohexan-1-ol

: 385423-97-2
(2S,3S)-2,3-dimethylcyclohexanone

: 1174149-18-8
trans-1,2-dimethylcyclohexan-1-ol

: 75364-88-4
(3S,4R)-3,4-dimethylcyclohexanone

Guidance literature:: With C₃₃H₂₈FeN₆⁽²⁺⁾*2ClO₄^(1-); 2-iodylbenzoic acid 1-methylethyl ester; In acetonitrile; for 3h; Catalytic behavior;
DOI:10.1039/d1dt03381f

Reference yield:

: 160961-89-7
(S,S,S)-2,3-dimethyl-5-(2-propen-2-yl)-cyclohexanone

: 385423-97-2
(2S,3S)-2,3-dimethylcyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: O₃ / methanol / 1.5 h / -40 - -10 °C

1.2: 13 percent / Cu(OAc)2*H₂O; FeSO₄*7H₂O / methanol / 18 h / -20 - 20 °C

2.1: H₂ / 5percent Rh/C / petroleum ether / 3 h

With hydrogen; ozone; 5percent Rh/C; In methanol; Petroleum ether;
DOI:10.1002/1099-0690(200110)2001:20<3831::AID-EJOC3831>3.0.CO;2-2

Reference yield:

: (S,S)-5,6-dimethyl-3-cyclohexenone

: 385423-97-2
(2S,3S)-2,3-dimethylcyclohexanone

: cis-2,3-dimethylcyclohexan-1-one

Guidance literature:: With hydrogen; 5percent Rh/C; In Petroleum ether; for 3h; Title compound not separated from byproducts.;
DOI:10.1002/1099-0690(200110)2001:20<3831::AID-EJOC3831>3.0.CO;2-2