N-(2-Benzyloxy-6-bromo-5-ethyl-4-methoxy-3-methyl-phenyl)-N-methyl-acrylamide

Base Information

Chemical Name:N-(2-Benzyloxy-6-bromo-5-ethyl-4-methoxy-3-methyl-phenyl)-N-methyl-acrylamide
CAS No.:154492-42-9
Molecular Formula:C₂₁H₂₄BrNO₃
Molecular Weight:418.33
Hs Code.:

Synonyms:N-(2-Benzyloxy-6-bromo-5-ethyl-4-methoxy-3-methyl-phenyl)-N-methyl-acrylamide

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Chemical Property of N-(2-Benzyloxy-6-bromo-5-ethyl-4-methoxy-3-methyl-phenyl)-N-methyl-acrylamide

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Technology Process of N-(2-Benzyloxy-6-bromo-5-ethyl-4-methoxy-3-methyl-phenyl)-N-methyl-acrylamide

There total 8 articles about N-(2-Benzyloxy-6-bromo-5-ethyl-4-methoxy-3-methyl-phenyl)-N-methyl-acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 154492-41-8
N-(2-Benzyloxy-6-bromo-5-ethyl-4-methoxy-3-methyl-phenyl)-acrylamide

: 74-88-4
methyl iodide

: 154492-42-9
N-(2-Benzyloxy-6-bromo-5-ethyl-4-methoxy-3-methyl-phenyl)-N-methyl-acrylamide

Guidance literature:: With potassium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)61569-1

Reference yield:

: 118824-96-7
4'-Benzyloxy-2'-methoxy-3'-methylacetophenone

: 154492-42-9
N-(2-Benzyloxy-6-bromo-5-ethyl-4-methoxy-3-methyl-phenyl)-N-methyl-acrylamide

Guidance literature:: Multi-step reaction with 7 steps

1: hydrogen / palladium on charcoal / ethanol / 72 h

2: 86 percent / conc. nitric acid / acetic acid

3: 84 percent / potassium carbonate / acetone / Heating

4: 99 percent / tin II chloride

5: 92 percent / pyridinium hydrobromide perbromide / acetic acid

6: 96 percent

7: 90 percent / KH / tetrahydrofuran

With hydrogen; nitric acid; pyridinium hydrobromide perbromide; potassium hydride; potassium carbonate; tin(ll) chloride; palladium on activated charcoal; In tetrahydrofuran; ethanol; acetic acid; acetone;
DOI:10.1016/S0040-4039(00)61569-1

Reference yield:

: 100-39-0
benzyl bromide

: 154492-42-9
N-(2-Benzyloxy-6-bromo-5-ethyl-4-methoxy-3-methyl-phenyl)-N-methyl-acrylamide

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / potassium carbonate / acetone / Heating

2: 99 percent / tin II chloride

3: 92 percent / pyridinium hydrobromide perbromide / acetic acid

4: 96 percent

5: 90 percent / KH / tetrahydrofuran

With pyridinium hydrobromide perbromide; potassium hydride; potassium carbonate; tin(ll) chloride; In tetrahydrofuran; acetic acid; acetone;
DOI:10.1016/S0040-4039(00)61569-1