C₅₄H₄₄N₄O₄

Base Information

• Chemical Name: C₅₄H₄₄N₄O₄
• CAS No.: 181584-38-3
• Molecular Formula: C₅₄H₄₄N₄O₄
• Molecular Weight: 812.968
• Mol file: 181584-38-3.mol

Synonyms:C₅₄H₄₄N₄O₄

Chemical Property of C₅₄H₄₄N₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₄H₄₄N₄O₄

There total 10 articles about C₅₄H₄₄N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

1,6-bis[(8-propargylbenzyloxycarbonylamino)-6-phenanthridinyl]-hexane (181584-32-7) → C54H44N4O4 (181584-38-3)

Guidance literature:

With pyridine; copper diacetate; In acetonitrile; at 60 ℃; for 72h;

Reference yield:

2-(4-nitrophenyl)aniline (6272-52-2) → C54H44N4O4 (181584-38-3)

Guidance literature:

Multi-step reaction with 8 steps

1: 85 percent / benzene / 24 h / Heating

2: 100 percent / H₂ / 10percent Pd/C / dimethylformamide; ethanol / 15 h / 70 °C / 37503 Torr

3: 85 percent / N,N-dimethylaniline / ethanol / 6 h / Heating

4: 77 percent / POCl₃ / 2 h / Heating

5: 93 percent / 70percent aq. H₂SO₄ / 0.5 h / 140 °C

6: 87 percent / NaHCO₃ / toluene; dimethylformamide / 0.5 h / 0 °C

7: 65 percent / K₂CO₃ / toluene; dimethylformamide / 48 h / 45 °C

8: 49 percent / Cu(OAc)2*H₂O, pyridine / acetonitrile / 72 h / 60 °C

With pyridine; copper diacetate; sulfuric acid; hydrogen; sodium hydrogencarbonate; potassium carbonate; N,N-dimethyl-aniline; trichlorophosphate; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; toluene; acetonitrile; benzene;

Reference yield:

suberoyl chloride (10027-07-3) → C54H44N4O4 (181584-38-3)

Guidance literature:

Multi-step reaction with 8 steps

1: 85 percent / benzene / 24 h / Heating

2: 100 percent / H₂ / 10percent Pd/C / dimethylformamide; ethanol / 15 h / 70 °C / 37503 Torr

3: 85 percent / N,N-dimethylaniline / ethanol / 6 h / Heating

4: 77 percent / POCl₃ / 2 h / Heating

5: 93 percent / 70percent aq. H₂SO₄ / 0.5 h / 140 °C

6: 87 percent / NaHCO₃ / toluene; dimethylformamide / 0.5 h / 0 °C

7: 65 percent / K₂CO₃ / toluene; dimethylformamide / 48 h / 45 °C

8: 49 percent / Cu(OAc)2*H₂O, pyridine / acetonitrile / 72 h / 60 °C

With pyridine; copper diacetate; sulfuric acid; hydrogen; sodium hydrogencarbonate; potassium carbonate; N,N-dimethyl-aniline; trichlorophosphate; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; toluene; acetonitrile; benzene;

upstream raw materials:

1,6-bis[(8-propargylbenzyloxycarbonylamino)-6-phenanthridinyl]-hexane

2-(4-nitrophenyl)aniline

suberoyl chloride

benzyl chloroformate