(1R)-1-(phenylprop-2-enyl)-(1S)-1-[(phenylmethoxy)methyl]prop-2-enyl-[(4-methylphenyl)sulfonyl]amine

Base Information

Chemical Name:(1R)-1-(phenylprop-2-enyl)-(1S)-1-[(phenylmethoxy)methyl]prop-2-enyl-[(4-methylphenyl)sulfonyl]amine
CAS No.:255043-88-0
Molecular Formula:C₂₇H₂₉NO₃S
Molecular Weight:447.598
Hs Code.:

Synonyms:(1R)-1-(phenylprop-2-enyl)-(1S)-1-[(phenylmethoxy)methyl]prop-2-enyl-[(4-methylphenyl)sulfonyl]amine

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Chemical Property of (1R)-1-(phenylprop-2-enyl)-(1S)-1-[(phenylmethoxy)methyl]prop-2-enyl-[(4-methylphenyl)sulfonyl]amine

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Technology Process of (1R)-1-(phenylprop-2-enyl)-(1S)-1-[(phenylmethoxy)methyl]prop-2-enyl-[(4-methylphenyl)sulfonyl]amine

There total 5 articles about (1R)-1-(phenylprop-2-enyl)-(1S)-1-[(phenylmethoxy)methyl]prop-2-enyl-[(4-methylphenyl)sulfonyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 255043-86-8
(S)-N-(1-(benzyloxy)but-3-en-2-yl)-4-methylbenzenesulfonamide

: 255043-87-9
(R)-(+)-1-phenyl-prop-2-enyl methyl carbonate

: 255043-88-0
(1R)-1-(phenylprop-2-enyl)-(1S)-1-[(phenylmethoxy)methyl]prop-2-enyl-[(4-methylphenyl)sulfonyl]amine

: C₂₇H₂₉NO₃S

Guidance literature:: (S)-N-(1-(benzyloxy)but-3-en-2-yl)-4-methylbenzenesulfonamide; With lithium hexamethyldisilazane; In tetrahydrofuran; at 30 ℃; for 0.5h;

(R)-(+)-1-phenyl-prop-2-enyl methyl carbonate; With phosphorous acid trimethyl ester; tris(triphenylphosphine)rhodium(I) chloride; In tetrahydrofuran; at 30 ℃; for 6h; Further stages.;
DOI:10.1021/ol991064l

Reference yield:

: 255043-86-8
(S)-N-(1-(benzyloxy)but-3-en-2-yl)-4-methylbenzenesulfonamide

: 171037-07-3
(S)-(-)-1-phenyl-prop-2-enyl methyl carbonate

: 255043-88-0
(1R)-1-(phenylprop-2-enyl)-(1S)-1-[(phenylmethoxy)methyl]prop-2-enyl-[(4-methylphenyl)sulfonyl]amine

: C₂₇H₂₉NO₃S

: 255043-89-1
C₂₇H₂₉NO₃S

Guidance literature:: (S)-N-(1-(benzyloxy)but-3-en-2-yl)-4-methylbenzenesulfonamide; With lithium hexamethyldisilazane; In tetrahydrofuran; at 30 ℃;

(S)-(-)-1-phenyl-prop-2-enyl methyl carbonate; With phosphorous acid trimethyl ester; tris(triphenylphosphine)rhodium(I) chloride; In tetrahydrofuran; at 30 ℃; Further stages.;
DOI:10.1021/ol991064l

Reference yield:

: C₁₅H₁₆SO₃N^(1-)*Li⁽¹⁺⁾

: 255043-88-0
(1R)-1-(phenylprop-2-enyl)-(1S)-1-[(phenylmethoxy)methyl]prop-2-enyl-[(4-methylphenyl)sulfonyl]amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethyl phosphite / RhCl(PPh₃)3 / tetrahydrofuran / 30 °C

2.1: 89 percent / trifluoroacetic acid / 20 °C

3.1: lithium hexamethyldisilylazide / tetrahydrofuran / 0.5 h / 30 °C

3.2: trimethyl phosphite / [Rh(PPh₃)3Cl] / tetrahydrofuran / 6 h / 30 °C

With trifluoroacetic acid; lithium hexamethyldisilazane; phosphorous acid trimethyl ester; RhCl(PPh₃)3; In tetrahydrofuran;
DOI:10.1021/ol991064l