N₃-(2,6-dimethylphenyl)-1-(2-(oxiran-2-yl)ethyl)-N₆-phenyl-1H-pyrazolo[3,4-d]pyrimidine-3,6-diamine

Base Information

• Chemical Name: N₃-(2,6-dimethylphenyl)-1-(2-(oxiran-2-yl)ethyl)-N₆-phenyl-1H-pyrazolo[3,4-d]pyrimidine-3,6-diamine
• CAS No.: 927681-12-7
• Molecular Formula: C₂₃H₂₄N₆O
• Molecular Weight: 400.483

Synonyms:N₃-(2,6-dimethylphenyl)-1-(2-(oxiran-2-yl)ethyl)-N₆-phenyl-1H-pyrazolo[3,4-d]pyrimidine-3,6-diamine

Chemical Property of N₃-(2,6-dimethylphenyl)-1-(2-(oxiran-2-yl)ethyl)-N₆-phenyl-1H-pyrazolo[3,4-d]pyrimidine-3,6-diamine

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Technology Process of N₃-(2,6-dimethylphenyl)-1-(2-(oxiran-2-yl)ethyl)-N₆-phenyl-1H-pyrazolo[3,4-d]pyrimidine-3,6-diamine

There total 2 articles about N₃-(2,6-dimethylphenyl)-1-(2-(oxiran-2-yl)ethyl)-N₆-phenyl-1H-pyrazolo[3,4-d]pyrimidine-3,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C30H32N6O4S → N3-(2,6-dimethylphenyl)-1-(2-(oxiran-2-yl)ethyl)-N6-phenyl-1H-pyrazolo[3,4-d]pyrimidine-3,6-diamine (927681-12-7)

Guidance literature:

With sodium methylate; In methanol; chloroform; at 0 ℃;

DOI:10.1016/j.bmcl.2008.10.092

Reference yield:

4-(3-(2,6-dimethylphenylamino)-6-(phenylamino)-1H-pyrazolo[3,4-d]pyrimidin-1-yl)butane-1,2-diol (927680-65-7) → N3-(2,6-dimethylphenyl)-1-(2-(oxiran-2-yl)ethyl)-N6-phenyl-1H-pyrazolo[3,4-d]pyrimidine-3,6-diamine (927681-12-7)

Guidance literature:

4-(3-(2,6-dimethylphenylamino)-6-(phenylamino)-1H-pyrazolo[3,4-d]pyrimidin-1-yl)butane-1,2-diol; With pyridine; p-toluenesulfonyl chloride; In dichloromethane; at 20 ℃; for 23.5h;

With sodium methylate; In methanol; chloroform; at 0 ℃; for 0.833333h;

Reference yield: 27.0%

N3-(2,6-dimethylphenyl)-1-(2-(oxiran-2-yl)ethyl)-N6-phenyl-1H-pyrazolo[3,4-d]pyrimidine-3,6-diamine (927681-12-7) + methylamine (74-89-5) → C25H31N7O

Guidance literature:

With ethanol; at 40 ℃;

DOI:10.1016/j.bmcl.2008.10.092

upstream raw materials:

4-(3-(2,6-dimethylphenylamino)-6-(phenylamino)-1H-pyrazolo[3,4-d]pyrimidin-1-yl)butane-1,2-diol

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