2-deuterio-2-phenyloxirane

Base Information

Chemical Name:2-deuterio-2-phenyloxirane
CAS No.:52881-58-0
Molecular Formula:C₈H₈O
Molecular Weight:121.143
Hs Code.:

Synonyms:2-deuterio-2-phenyloxirane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-deuterio-2-phenyloxirane

Chemical Property:

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Technology Process of 2-deuterio-2-phenyloxirane

There total 5 articles about 2-deuterio-2-phenyloxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 70-11-1
α-bromoacetophenone

: 52881-58-0
2-deuterio-2-phenyloxirane

Guidance literature:: α-bromoacetophenone; With sodium borodeuteride; In methanol; at 0 - 20 ℃; for 3h; Schlenk technique; Inert atmosphere;

With potassium tert-butylate; for 20h;
DOI:10.1021/acs.joc.8b01374

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1193-80-2
α-deuteriostyrene

: 96-09-3
styrene oxide

: 52881-58-0
2-deuterio-2-phenyloxirane

Guidance literature:: styrene; α-deuteriostyrene; With Pyridine-2,6-dicarboxylic acid; iron(III) chloride hexahydrate; C₂₈H₂₈N₂O₂S; In tert-Amyl alcohol; at 20 ℃;

With dihydrogen peroxide; In tert-Amyl alcohol; water; at 20 ℃; for 1h; Reactivity;
DOI:10.1002/chem.200800595

Reference yield:

: 1193-80-2
α-deuteriostyrene

: 52881-58-0
2-deuterio-2-phenyloxirane

Guidance literature:: With {Ru(2,2':6',2''-terpyridine)(N,N,N',N'tetramethylethylenediamine)O}(ClO₄)2; In acetonitrile; at 25 ℃; for 12h; Rate constant; other reagents, kinetic isotope effect;
DOI:10.1021/jo980755c