2,6-bis{1-[(2-isopropylphenyl)imino]ethyl}pyridine

Base Information

Chemical Name:2,6-bis{1-[(2-isopropylphenyl)imino]ethyl}pyridine
CAS No.:210537-34-1
Molecular Formula:C₂₇H₃₁N₃
Molecular Weight:397.563
Hs Code.:

Synonyms:2,6-bis{1-[(2-isopropylphenyl)imino]ethyl}pyridine

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Chemical Property of 2,6-bis{1-[(2-isopropylphenyl)imino]ethyl}pyridine

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Technology Process of 2,6-bis{1-[(2-isopropylphenyl)imino]ethyl}pyridine

There total 2 articles about 2,6-bis{1-[(2-isopropylphenyl)imino]ethyl}pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1129-30-2
2,6-Diacetylpyridine

: 643-28-7
2-isopropylaniline

: 210537-34-1
2,6-bis{1-[(2-isopropylphenyl)imino]ethyl}pyridine

: 2-acetyl-6-[1-((2-isopropylphenyl)imino)ethyl]pyridine

Guidance literature:: With magnesium sulfate; toluene-4-sulfonic acid; In neat (no solvent); at 21 - 23 ℃; for 4h; Sealed tube; Milling;
DOI:10.1039/c8dt03608j

Reference yield:

: 1129-30-2
2,6-Diacetylpyridine

: 643-28-7
2-isopropylaniline

: 210537-34-1
2,6-bis{1-[(2-isopropylphenyl)imino]ethyl}pyridine

Guidance literature:: In dichloromethane; Acidic conditions;
DOI:10.1016/j.ica.2011.03.047

Reference yield: 99.0%

: 210537-34-1
2,6-bis{1-[(2-isopropylphenyl)imino]ethyl}pyridine

: cobalt(II) chloride hexahydrate

: 590367-46-7
2,6-bis[1-(2-isopropylphenylimino)ethyl]pyridinecobalt(II) chloride

Guidance literature:: In tetrahydrofuran; stirring a slight excess of the ligand with CoCl2*6H2O in THF for at least 1 day; adding pentane to soln.; filtration; heating under vac. at 40 °C;elem. anal.;
DOI:10.1021/om030210v