(3R,4R,5R)-5-benzyloxy-6-(1,3-dithian-2-yl)-4-methoxy-2-methyl-3-hexanol

Base Information

Chemical Name:(3R,4R,5R)-5-benzyloxy-6-(1,3-dithian-2-yl)-4-methoxy-2-methyl-3-hexanol
CAS No.:160238-69-7
Molecular Formula:C₁₉H₃₀O₃S₂
Molecular Weight:370.577
Hs Code.:

Synonyms:(3R,4R,5R)-5-benzyloxy-6-(1,3-dithian-2-yl)-4-methoxy-2-methyl-3-hexanol

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Chemical Property of (3R,4R,5R)-5-benzyloxy-6-(1,3-dithian-2-yl)-4-methoxy-2-methyl-3-hexanol

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Technology Process of (3R,4R,5R)-5-benzyloxy-6-(1,3-dithian-2-yl)-4-methoxy-2-methyl-3-hexanol

There total 3 articles about (3R,4R,5R)-5-benzyloxy-6-(1,3-dithian-2-yl)-4-methoxy-2-methyl-3-hexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 109-80-8
1.3-propanedithiol

: 160238-68-6
(2R,3S,4R,6S)-4-benzyloxy-2-isopropyl-3,6-dimethoxy-3,4,5,6-tetrahydro-2H-pyran

: 160238-69-7
(3R,4R,5R)-5-benzyloxy-6-(1,3-dithian-2-yl)-4-methoxy-2-methyl-3-hexanol

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/0040-4020(96)00811-3

Reference yield:

: 100-39-0
benzyl bromide

: 160238-69-7
(3R,4R,5R)-5-benzyloxy-6-(1,3-dithian-2-yl)-4-methoxy-2-methyl-3-hexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaH / tetrahydrofuran; dimethylformamide / 12 h / Ambient temperature

2: 81 percent / BF₃*Et₂O / CH₂Cl₂ / 24 h / Ambient temperature

With boron trifluoride diethyl etherate; sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(96)00811-3

Reference yield:

: 160238-67-5
(2R,3S,4R,6S)-2-isopropyl-3,6-dimethoxy-3,4,5,6-tetrahydro-2H-pyran-4-ol

: 160238-69-7
(3R,4R,5R)-5-benzyloxy-6-(1,3-dithian-2-yl)-4-methoxy-2-methyl-3-hexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaH / tetrahydrofuran; dimethylformamide / 12 h / Ambient temperature

2: 81 percent / BF₃*Et₂O / CH₂Cl₂ / 24 h / Ambient temperature

With boron trifluoride diethyl etherate; sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(96)00811-3