2-[(phenylmethyl)oxy]-N-3-pyridinyl-5-(1-pyrrolidinylcarbonyl)benzamide

Base Information

Chemical Name:2-[(phenylmethyl)oxy]-N-3-pyridinyl-5-(1-pyrrolidinylcarbonyl)benzamide
CAS No.:1285513-94-1
Molecular Formula:C₂₄H₂₃N₃O₃
Molecular Weight:401.465
Hs Code.:

Synonyms:2-[(phenylmethyl)oxy]-N-3-pyridinyl-5-(1-pyrrolidinylcarbonyl)benzamide

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Chemical Property of 2-[(phenylmethyl)oxy]-N-3-pyridinyl-5-(1-pyrrolidinylcarbonyl)benzamide

Chemical Property:

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Technology Process of 2-[(phenylmethyl)oxy]-N-3-pyridinyl-5-(1-pyrrolidinylcarbonyl)benzamide

There total 7 articles about 2-[(phenylmethyl)oxy]-N-3-pyridinyl-5-(1-pyrrolidinylcarbonyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 462-08-8
pyridin-3-ylamine

: 1285516-57-5
2-[(phenylmethyl)oxy]-5-(1-pyrrolidinylcarbonyl)benzoic acid

: 1285513-94-1
2-[(phenylmethyl)oxy]-N-3-pyridinyl-5-(1-pyrrolidinylcarbonyl)benzamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 4h; Inert atmosphere;

Reference yield:

: 636-46-4
4-hydroxyisophthalic acid

: 1285513-94-1
2-[(phenylmethyl)oxy]-N-3-pyridinyl-5-(1-pyrrolidinylcarbonyl)benzamide

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / acetone / 50 °C

2: water; lithium hydroxide / tetrahydrofuran / 20 °C

3: sulfuric acid / 3 h / 20 °C

4: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

5: dichloromethane / 2 h / 20 °C

6: water; lithium hydroxide / tetrahydrofuran / 3 h / 20 °C

7: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

With oxalyl dichloride; sulfuric acid; water; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1285516-43-9
bis(phenylmethyl) 4-[(phenylmethyl)oxy]-1,3-benzenedicarboxylate

: 1285513-94-1
2-[(phenylmethyl)oxy]-N-3-pyridinyl-5-(1-pyrrolidinylcarbonyl)benzamide

Guidance literature:: Multi-step reaction with 6 steps

1: water; lithium hydroxide / tetrahydrofuran / 20 °C

2: sulfuric acid / 3 h / 20 °C

3: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

4: dichloromethane / 2 h / 20 °C

5: water; lithium hydroxide / tetrahydrofuran / 3 h / 20 °C

6: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

With oxalyl dichloride; sulfuric acid; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;