P-DIMETHYLAMINOBENZYLIDENE P-ANISIDINE

Base Information

• Chemical Name: P-DIMETHYLAMINOBENZYLIDENE P-ANISIDINE
• CAS No.: 1749-04-8
• Molecular Formula: C16H18 N2 O
• Molecular Weight: 254.332
• Hs Code.: 2925290090
• Mol file: 1749-04-8.mol

Synonyms:p-Anisidine,N-[p-(dimethylamino)benzylidene]- (7CI,8CI);N-(4-Dimethylaminobenzylidene)-p-anisidine; p-Dimethylaminobenzal-p-anisidine;p-Dimethylaminobenzal-p'-anisidine

Chemical Property of P-DIMETHYLAMINOBENZYLIDENE P-ANISIDINE

Chemical Property:

• Vapor Pressure: 5.39E-07mmHg at 25°C
• Boiling Point: 411.9°C at 760 mmHg
• Flash Point: 202.9°C
• PSA: 24.83000
• Density: 1g/cm³
• LogP: 3.51180

Purity/Quality:

99% ^*data from raw suppliers

p-Dimethylaminobenzylidene p-anisidine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of P-DIMETHYLAMINOBENZYLIDENE P-ANISIDINE

There total 5 articles about P-DIMETHYLAMINOBENZYLIDENE P-ANISIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-methoxy-aniline (104-94-9) + 4-dimethylamino-benzaldehyde (100-10-7) → N-(4-(N,N-dimethylamino)benzal)-p-anisidine (1749-04-8)

Guidance literature:

With sulfuric acid; In neat (no solvent); Microwave irradiation; Sealed tube; Green chemistry;

DOI:10.1016/j.saa.2012.09.039

Reference yield:

4-methoxy-benzoyl chloride (100-07-2) → N-(4-(N,N-dimethylamino)benzal)-p-anisidine (1749-04-8)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene; sodium azide

With sodium azide; toluene;

Reference yield:

4-Methoxyphenyl isocyanate (5416-93-3) + 4-dimethylamino-benzaldehyde (100-10-7) → N-(4-(N,N-dimethylamino)benzal)-p-anisidine (1749-04-8)

Guidance literature:

upstream raw materials:

4-methoxy-aniline

4-dimethylamino-benzaldehyde

4-Methoxyphenyl isocyanate

1-(4-cyanophenyl)-3-(4-dimethylaminophenyl)-prop-2-ene-1-one

Downstream raw materials:

2,5-di(p-anisyl)amino-3,6-dibromo-1,4-benzoquinone

C₁₆H₁₈N₂O*C₂HCl₃O₂

2-chloro-3-(4-methoxyphenyl)amino-1,4-naphthoquinone

4-dimethylamino-benzaldehyde

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