methyl 1-(3-chloro-4-(α-D-mannopyranosyloxy)phenyl)-1H-indole-5-carboxylate

Base Information

Chemical Name:methyl 1-(3-chloro-4-(α-D-mannopyranosyloxy)phenyl)-1H-indole-5-carboxylate
CAS No.:1312312-53-0
Molecular Formula:C₂₂H₂₂ClNO₈
Molecular Weight:463.872
Hs Code.:

Synonyms:methyl 1-(3-chloro-4-(α-D-mannopyranosyloxy)phenyl)-1H-indole-5-carboxylate

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Chemical Property of methyl 1-(3-chloro-4-(α-D-mannopyranosyloxy)phenyl)-1H-indole-5-carboxylate

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Technology Process of methyl 1-(3-chloro-4-(α-D-mannopyranosyloxy)phenyl)-1H-indole-5-carboxylate

There total 4 articles about methyl 1-(3-chloro-4-(α-D-mannopyranosyloxy)phenyl)-1H-indole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1312312-52-9
benzyl 1-(3-chloro-4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl)-1H-indole-5-carboxylate

: 124-41-4
sodium methylate

: 1312312-53-0
methyl 1-(3-chloro-4-(α-D-mannopyranosyloxy)phenyl)-1H-indole-5-carboxylate

Guidance literature:: benzyl 1-(3-chloro-4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl)-1H-indole-5-carboxylate; sodium methylate; In methanol; at 20 ℃;

With amberlyst-15; In methanol;

Reference yield:

: 116130-33-7
2-chloro-4-iodophenol

: 1312312-53-0
methyl 1-(3-chloro-4-(α-D-mannopyranosyloxy)phenyl)-1H-indole-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylsilyl trifluoromethanesulfonate / toluene / 2 h / 20 °C / Inert atmosphere; Molecular sieve

2.1: potassium phosphate; trans cyclohexane-1,2-diamine / 1,4-dioxane / 105 °C / Inert atmosphere; Sealed tube

2.2: 2 h / Inert atmosphere; Sealed tube

3.1: sodium methylate / 20 °C

With potassium phosphate; trans cyclohexane-1,2-diamine; trimethylsilyl trifluoromethanesulfonate; sodium methylate; In 1,4-dioxane; toluene;
DOI:10.1021/jm300192x

Reference yield:

: 1312312-40-5
2-chloro-4-iodophenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

: 1312312-53-0
methyl 1-(3-chloro-4-(α-D-mannopyranosyloxy)phenyl)-1H-indole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium phosphate; trans cyclohexane-1,2-diamine / 1,4-dioxane / 105 °C / Inert atmosphere; Sealed tube

1.2: 2 h / Inert atmosphere; Sealed tube

2.1: sodium methylate / 20 °C

With potassium phosphate; trans cyclohexane-1,2-diamine; sodium methylate; In 1,4-dioxane;
DOI:10.1021/jm300192x