Ph₂Pt((4-Br-2,6-Me₃C₆H₂)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me₂C₆H₂))

Base Information

Chemical Name:Ph₂Pt((4-Br-2,6-Me₃C₆H₂)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me₂C₆H₂))
CAS No.:881910-76-5
Molecular Formula:C₃₂H₃₂Br₂N₂Pt
Molecular Weight:799.507
Hs Code.:

Ph<sub>2</sub>Pt((4-Br-2,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me<sub>2</sub>C<sub>6</sub>H<sub>2</sub>))

Synonyms:Ph₂Pt((4-Br-2,6-Me₃C₆H₂)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me₂C₆H₂))

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Chemical Property of Ph₂Pt((4-Br-2,6-Me₃C₆H₂)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me₂C₆H₂))

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Technology Process of Ph₂Pt((4-Br-2,6-Me₃C₆H₂)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me₂C₆H₂))

There total 1 articles about Ph₂Pt((4-Br-2,6-Me₃C₆H₂)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me₂C₆H₂)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: cis-(PtPh₂(SMe₂)2)

: 181709-92-2
1,4-bis(2,6-dimethyl-4-bromophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

: 881910-76-5
Ph₂Pt((4-Br-2,6-Me₃C₆H₂)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me₂C₆H₂))

Guidance literature:: In toluene; diimine added to soln. of Pt complex in toluene; mixt. stirred for 18 h; solvent removed (vac.); residue dissolved (CH2Cl2); filtered; pentane added; solvent decanted; dried (vac.); elem. anal.;
DOI:10.1021/ja056694z

Reference yield:

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 881910-76-5
Ph₂Pt((4-Br-2,6-Me₃C₆H₂)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me₂C₆H₂))

: 881910-97-0
[Ph(η2-C6H6)Pt((4-Br-2,6-Me3C6H2)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me2C6H2))][BF4]

Guidance literature:: In dichloromethane-d2; soln. of Pt complex in CD2Cl2 was carefully layered with CD2Cl2; cooled to -78°C; layered with soln. of HBF4*Et2O in a mixt. of Et2O-d10 and CD2Cl2; tube was capped and kept at -78°C; not isolated; monitored by NMR spectroscopy;
DOI:10.1021/ja056694z

Reference yield:

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 2206-26-0
[D₃]acetonitrile

: 881910-76-5
Ph₂Pt((4-Br-2,6-Me₃C₆H₂)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me₂C₆H₂))

: 881910-85-6
[Ph(acetonitrile-d3)Pt((4-Br-2,6-Me₂C₆H₂)-N=C(Me)-C(Me)=N-(4-Br-2,6-Me₂C₆H₂))][BF₄]

Guidance literature:: In dichloromethane-d2; [D₃]acetonitrile; byproducts: C6H6; HBF4*Et2O added to NMR tube contg. CD2Cl2 with added CD3CN; not isolated; monitored by NMR spectroscopy;
DOI:10.1021/ja056694z