Technology Process of 1-iodo-2,4-dimethoxymethoxybenzene
There total 2 articles about 1-iodo-2,4-dimethoxymethoxybenzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iodine; silver(I) acetate;
In
chloroform;
at 20 ℃;
for 5h;
regiospecific reaction;
Inert atmosphere;
DOI:10.1016/j.tet.2011.09.042
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: acetyl chloride; zinc dibromide / dichloromethane / 3 h / 20 °C / Inert atmosphere
1.2: 3 h / Inert atmosphere; Cooling with ice
2.1: iodine; silver(I) acetate / chloroform / 5 h / 20 °C / Inert atmosphere
With
iodine; silver(I) acetate; acetyl chloride; zinc dibromide;
In
dichloromethane; chloroform;
DOI:10.1016/j.tet.2011.09.042
- Guidance literature:
-
With
cesium phosphate; palladium(II) trifluoroacetate;
In
tert-Amyl alcohol; water;
at 110 ℃;
for 72h;
Reagent/catalyst;
Temperature;
Catalytic behavior;
Inert atmosphere;
Sealed tube;
DOI:10.1039/c6ob00110f
