Technology Process of C27H34ClFN6O5S
There total 12 articles about C27H34ClFN6O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap;
In
acetonitrile;
at 50 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 - 5 °C
1.2: 1 h / 75 °C
2.1: copper diacetate; pyridine / dichloromethane / 16 h / 23 °C
3.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol / 6 h / 23 °C
4.1: dmap / acetonitrile / 50 °C
With
pyridine; hydrogenchloride; dmap; palladium 10% on activated carbon; hydrogen; copper diacetate; sodium nitrite;
In
methanol; dichloromethane; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydride / paraffin oil; 1,4-dioxane / 0.75 h
1.2: 3 h / Reflux
2.1: hydrazine hydrate / ethanol / 3 h / Reflux
3.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 - 5 °C
3.2: 1 h / 75 °C
4.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 23 °C
4.2: 0.5 h / 100 °C
5.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol / 6 h / 23 °C
6.1: dmap / acetonitrile / 50 °C
With
hydrogenchloride; dmap; palladium 10% on activated carbon; hydrogen; sodium hydride; hydrazine hydrate; sodium nitrite;
In
1,4-dioxane; methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile; paraffin oil;