2-(N-(2-fluoro-4-(phenoxycarbonylamino)benzyl)sulfamoyl-carbamoyloxy)-2-methylpropan-1-ylium

Base Information

Chemical Name:2-(N-(2-fluoro-4-(phenoxycarbonylamino)benzyl)sulfamoyl-carbamoyloxy)-2-methylpropan-1-ylium
CAS No.:1402586-22-4
Molecular Formula:C₁₉H₂₂FN₃O₆S
Molecular Weight:439.465
Hs Code.:

Synonyms:2-(N-(2-fluoro-4-(phenoxycarbonylamino)benzyl)sulfamoyl-carbamoyloxy)-2-methylpropan-1-ylium

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Chemical Property of 2-(N-(2-fluoro-4-(phenoxycarbonylamino)benzyl)sulfamoyl-carbamoyloxy)-2-methylpropan-1-ylium

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Technology Process of 2-(N-(2-fluoro-4-(phenoxycarbonylamino)benzyl)sulfamoyl-carbamoyloxy)-2-methylpropan-1-ylium

There total 2 articles about 2-(N-(2-fluoro-4-(phenoxycarbonylamino)benzyl)sulfamoyl-carbamoyloxy)-2-methylpropan-1-ylium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1402586-21-3
tert-butyl N-(4-amino-2-fluorobenzyl)sulfamoylcarbamate

: 1885-14-9
phenyl chloroformate

: 1402586-22-4
2-(N-(2-fluoro-4-(phenoxycarbonylamino)benzyl)sulfamoyl-carbamoyloxy)-2-methylpropan-1-ylium

Guidance literature:: With pyridine; In tetrahydrofuran; acetonitrile; at 0 - 20 ℃; for 1h;

Reference yield:

: 1402586-20-2
tert-butyl N-(2-fluoro-4-nitrobenzyl)sulfamoylcarbamate

: 1402586-22-4
2-(N-(2-fluoro-4-(phenoxycarbonylamino)benzyl)sulfamoyl-carbamoyloxy)-2-methylpropan-1-ylium

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium 10% on activated carbon / tetrahydrofuran; ethanol / 6 h / 20 °C

2: pyridine / tetrahydrofuran; acetonitrile / 1 h / 0 - 20 °C

With pyridine; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; ethanol; acetonitrile;