3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranosyl 1-diethyldithiocarbamate

Base Information

Chemical Name:3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranosyl 1-diethyldithiocarbamate
CAS No.:1563178-09-5
Molecular Formula:C₃₈H₅₃NO₅S₂Si
Molecular Weight:696.06
Hs Code.:

Synonyms:3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranosyl 1-diethyldithiocarbamate

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Chemical Property of 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranosyl 1-diethyldithiocarbamate

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Technology Process of 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranosyl 1-diethyldithiocarbamate

There total 2 articles about 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranosyl 1-diethyldithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 994-30-9
triethylsilyl chloride

: 1380516-32-4
3,4,6-tri-O-benzyl-β-D-glucopyranosyl 1-diethyldithiocarbamate

: 1563178-09-5
3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranosyl 1-diethyldithiocarbamate

Guidance literature:: With 1H-imidazole; In tetrahydrofuran; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jo500032k

Reference yield:

: 1518-58-7
diethylammonium diethyldithiocarbamate

: 1563178-09-5
3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranosyl 1-diethyldithiocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere

2: 1H-imidazole / tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; In tetrahydrofuran; methanol;
DOI:10.1021/jo500032k

Reference yield:

: 1563178-09-5
3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranosyl 1-diethyldithiocarbamate

: 67-63-0,8013-70-5
isopropyl alcohol

: 1563178-11-9
isopropyl 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranoside

: 1563178-10-8
isopropyl 3,4,6-tri-O-benzyl-2-O-triethylsilyl-α-D-glucopyranoside

Guidance literature:: 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranosyl 1-diethyldithiocarbamate; In dichloromethane; 1,2-dichloro-ethane; at 20 ℃; for 1h; Inert atmosphere; Molecular sieve;

isopropyl alcohol; With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; 1,2-dichloro-ethane; at -50 - -30 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo500032k