(10,10-dimethyl-5-(pyridin-2-yl)-6-azatricyclo[7.1.1.0^2,7]undeca-2⁽⁷⁾,3,5-trien-8-yl)diphenylmethanol

Base Information

• Chemical Name: (10,10-dimethyl-5-(pyridin-2-yl)-6-azatricyclo[7.1.1.0^2,7]undeca-2⁽⁷⁾,3,5-trien-8-yl)diphenylmethanol
• CAS No.: 1142279-31-9
• Molecular Formula: C₃₀H₂₈N₂O
• Molecular Weight: 432.565

Synonyms:(10,10-dimethyl-5-(pyridin-2-yl)-6-azatricyclo[7.1.1.0^2,7]undeca-2⁽⁷⁾,3,5-trien-8-yl)diphenylmethanol

Chemical Property of (10,10-dimethyl-5-(pyridin-2-yl)-6-azatricyclo[7.1.1.0^2,7]undeca-2⁽⁷⁾,3,5-trien-8-yl)diphenylmethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (10,10-dimethyl-5-(pyridin-2-yl)-6-azatricyclo[7.1.1.0^2,7]undeca-2⁽⁷⁾,3,5-trien-8-yl)diphenylmethanol

There total 3 articles about (10,10-dimethyl-5-(pyridin-2-yl)-6-azatricyclo[7.1.1.0^2,7]undeca-2⁽⁷⁾,3,5-trien-8-yl)diphenylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

benzophenone (119-61-9) + 10,10-dimethyl-5-pyridin-2-yl-6-aza-tricyclo[7.1.1.0(2,7)]-undeca-2(7),3,5-triene (144176-22-7) → (10,10-dimethyl-5-(pyridin-2-yl)-6-azatricyclo[7.1.1.02,7]undeca-2(7),3,5-trien-8-yl)diphenylmethanol (1142279-31-9)

Guidance literature:

10,10-dimethyl-5-pyridin-2-yl-6-aza-tricyclo[7.1.1.0(2,7)]-undeca-2⁽⁷⁾,3,5-triene; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;

benzophenone; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3h; Inert atmosphere;

DOI:10.1002/adsc.201100023

Reference yield:

1-(2-oxo-2-(2-pyridyl)ethyl)pyridinium iodide (26482-00-8) → (10,10-dimethyl-5-(pyridin-2-yl)-6-azatricyclo[7.1.1.02,7]undeca-2(7),3,5-trien-8-yl)diphenylmethanol (1142279-31-9)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium acetate; acetic acid / 100 °C

2: lithium diisopropyl amide / tetrahydrofuran / -78 °C

With ammonium acetate; acetic acid; lithium diisopropyl amide; In tetrahydrofuran;

DOI:10.1039/c8ra09575b

Reference yield:

pinocarvone (34413-88-2) → (10,10-dimethyl-5-(pyridin-2-yl)-6-azatricyclo[7.1.1.02,7]undeca-2(7),3,5-trien-8-yl)diphenylmethanol (1142279-31-9)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium acetate; acetic acid / 100 °C

2: lithium diisopropyl amide / tetrahydrofuran / -78 °C

With ammonium acetate; acetic acid; lithium diisopropyl amide; In tetrahydrofuran;

DOI:10.1039/c8ra09575b

upstream raw materials:

benzophenone

10,10-dimethyl-5-pyridin-2-yl-6-aza-tricyclo[7.1.1.0(2,7)]-undeca-2⁽⁷⁾,3,5-triene

pinocarvone

1-(2-oxo-2-(2-pyridyl)ethyl)pyridinium iodide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1142279-31-9 (10,10-dimethyl-5-(pyridin-2-yl)-6-azatricyclo[7.1.1.0^2,7]undeca-2⁽⁷⁾,3,5-trien-8-yl)diphenylmethanol

Send

Send

Metric Ton KG G Pound L ML

Send

Send