trans-2,3-Bispiperazine dibromide

Base Information

• Chemical Name: trans-2,3-Bispiperazine dibromide
• CAS No.: 103229-15-8
• Molecular Formula: 2Br*C₄₂H₄₂N₂P₂
• Molecular Weight: 796.564
• Mol file: 103229-15-8.mol

Synonyms:trans-2,3-Bispiperazine dibromide

Chemical Property of trans-2,3-Bispiperazine dibromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-2,3-Bispiperazine dibromide

There total 1 articles about trans-2,3-Bispiperazine dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

C40H34P2(2+)*Br(1-) (86671-49-0,91413-26-2) + ethylenediamine (107-15-3,85404-18-8) → trans-2,3-Bispiperazine dibromide (103229-15-8)

Guidance literature:

In chloroform; at 20 ℃; for 4h;

DOI:10.1055/s-1986-31476

Reference yield:

trans-2,3-Bispiperazine dibromide (103229-15-8) + benzaldehyde (100-52-7) → (2R,3R)-2-((E)-Styryl)-3-((Z)-styryl)-piperazine + (2R,3R)-2,3-Bis-((E)-styryl)-piperazine

Guidance literature:

With potassium tert-butylate; Multistep reaction. Title compound not separated from byproducts; 1.) ether, 20 deg C, 30 min; 2.) room temp., 15 h;

DOI:10.1055/s-1986-31476

Reference yield:

trans-2,3-Bispiperazine dibromide (103229-15-8) + benzaldehyde (100-52-7) → (2R,3R)-2-((E)-Styryl)-3-((Z)-styryl)-piperazine; hydrobromide + (2R,3R)-2,3-Bis-((E)-styryl)-piperazine; hydrobromide

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1055/s-1986-31476

upstream raw materials:

C₄₀H₃₄P₂⁽²⁺⁾*Br^(1-)

ethylenediamine