SX-628

Base Information

Chemical Name:SX-628
CAS No.:1360598-87-3
Molecular Formula:C₂₀H₁₉BFN₃O₃
Molecular Weight:379.199
Hs Code.:

Synonyms:SX-628

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Chemical Property of SX-628

Chemical Property:

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Technology Process of SX-628

There total 5 articles about SX-628 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1360598-96-4
C₂₆H₂₉BFN₃O₃

: 1360598-87-3
SX-628

Guidance literature:: C₂₆H₂₉BFN₃O₃; With potassium hydrogenfluoride; In methanol; at 20 ℃;

With chloro-trimethyl-silane; water; In acetonitrile; at 20 ℃; for 2h;

Reference yield:

: 371-40-4
4-fluoroaniline

: 1360598-87-3
SX-628

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

2.1: triethylamine / N,N-dimethyl-formamide / 48 h / 130 °C / Inert atmosphere

3.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 41 h / 80 °C / Sealed tube; Inert atmosphere

4.1: potassium hydrogenfluoride / methanol / 20 °C

4.2: 2 h / 20 °C

With potassium hydrogenfluoride; potassium acetate; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 442134-70-5
6-bromo-N-(4-fluoro-phenyl)-nicotinamide

: 1360598-87-3
SX-628

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / N,N-dimethyl-formamide / 48 h / 130 °C / Inert atmosphere

2.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 41 h / 80 °C / Sealed tube; Inert atmosphere

3.1: potassium hydrogenfluoride / methanol / 20 °C

3.2: 2 h / 20 °C

With potassium hydrogenfluoride; potassium acetate; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In methanol; N,N-dimethyl-formamide;