2-(4-chloro-5-methyl-2-mercaptobenzenesulfonylimino)-5,5-dimethylhexahydropyrimidine

Base Information

• Chemical Name: 2-(4-chloro-5-methyl-2-mercaptobenzenesulfonylimino)-5,5-dimethylhexahydropyrimidine
• CAS No.: 188717-81-9
• Molecular Formula: C₁₃H₁₈ClN₃O₂S₂
• Molecular Weight: 347.89

Synonyms:2-(4-chloro-5-methyl-2-mercaptobenzenesulfonylimino)-5,5-dimethylhexahydropyrimidine

Chemical Property of 2-(4-chloro-5-methyl-2-mercaptobenzenesulfonylimino)-5,5-dimethylhexahydropyrimidine

Chemical Property:

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Technology Process of 2-(4-chloro-5-methyl-2-mercaptobenzenesulfonylimino)-5,5-dimethylhexahydropyrimidine

There total 1 articles about 2-(4-chloro-5-methyl-2-mercaptobenzenesulfonylimino)-5,5-dimethylhexahydropyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

2,2-Dimethyl-1,3-diaminopropane (7328-91-8) + 6-chloro-7-methyl-3-methylthio-1,4,2-benzodithiazin 1,1-dioxide → 2-(4-chloro-5-methyl-2-mercaptobenzenesulfonylimino)-5,5-dimethylhexahydropyrimidine (188717-81-9) + C26H34Cl2N6O4S4

Guidance literature:

In methanol; for 26h; Ambient temperature;

Reference yield: 90.0%

2-(4-chloro-5-methyl-2-mercaptobenzenesulfonylimino)-5,5-dimethylhexahydropyrimidine (188717-81-9) → C26H34Cl2N6O4S4

Guidance literature:

With dimethyl sulfoxide; at 80 ℃; for 8h;

Reference yield: 81.0%

bromoacetic acid (79-08-3) + 2-(4-chloro-5-methyl-2-mercaptobenzenesulfonylimino)-5,5-dimethylhexahydropyrimidine (188717-81-9) → [5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-acetic acid (188718-94-7)

Guidance literature:

With sodium hydroxide; sodium carbonate; In water; at 80 - 85 ℃; for 2h;

upstream raw materials:

2,2-Dimethyl-1,3-diaminopropane

Downstream raw materials:

[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-phenyl-acetic acid

2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid

[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-acetic acid

2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid methyl ester

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