[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-acetic acid

Base Information

Chemical Name:[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-acetic acid
CAS No.:188718-94-7
Molecular Formula:C₁₅H₂₀ClN₃O₄S₂
Molecular Weight:405.926
Hs Code.:

Synonyms:[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-acetic acid

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Chemical Property of [5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-acetic acid

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Technology Process of [5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-acetic acid

There total 1 articles about [5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 79-08-3
bromoacetic acid

: 188717-81-9
2-(4-chloro-5-methyl-2-mercaptobenzenesulfonylimino)-5,5-dimethylhexahydropyrimidine

: 188718-94-7
[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-acetic acid

Guidance literature:: With sodium hydroxide; sodium carbonate; In water; at 80 - 85 ℃; for 2h;

Reference yield: 81.0%

: 67-56-1
methanol

: 188718-94-7
[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-acetic acid

: [5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-acetic acid methyl ester

Guidance literature:: With sulfuric acid; In methanol; for 70h; Heating;

Reference yield:

: 188718-94-7
[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-acetic acid

: 2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-N-(2-dimethylamino-ethyl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 98percent aq. H₂SO₄ / methanol / 70 h / Heating

2: 39 percent / toluene / 70 h / Heating

With sulfuric acid; In methanol; toluene;