2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid

Base Information

Chemical Name:2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid
CAS No.:188718-95-8
Molecular Formula:C₁₈H₂₆ClN₃O₄S₂
Molecular Weight:448.007
Hs Code.:

Synonyms:2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid

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Chemical Property of 2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid

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Technology Process of 2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid

There total 1 articles about 2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 584-93-0
2-Bromovaleric acid

: 188717-81-9
2-(4-chloro-5-methyl-2-mercaptobenzenesulfonylimino)-5,5-dimethylhexahydropyrimidine

: 188718-95-8
2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid

Guidance literature:: With sodium hydroxide; sodium carbonate; In water; at 80 - 85 ℃; for 2h;

Reference yield: 80.0%

: 67-56-1
methanol

: 188718-95-8
2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid

: 188719-03-1
2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid methyl ester

Guidance literature:: With sulfuric acid; In methanol; for 70h; Heating;

Reference yield:

: 188718-95-8
2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid

: 2-[5-Chloro-2-(5,5-dimethyl-tetrahydro-pyrimidin-2-ylidenesulfamoyl)-4-methyl-phenylsulfanyl]-pentanoic acid (2-dimethylamino-ethyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 98percent aq. H₂SO₄ / methanol / 70 h / Heating

2: 38 percent / toluene / 70 h / Heating

With sulfuric acid; In methanol; toluene;