C₁₃H₁₄BrNO

Base Information

Chemical Name:C₁₃H₁₄BrNO
CAS No.:1374961-75-7
Molecular Formula:C₁₃H₁₄BrNO
Molecular Weight:280.164
Hs Code.:

Synonyms:C₁₃H₁₄BrNO

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Chemical Property of C₁₃H₁₄BrNO

Chemical Property:

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Technology Process of C₁₃H₁₄BrNO

There total 5 articles about C₁₃H₁₄BrNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99299-09-9
(5-isopropyl-3-phenylisoxazol-4-yl)methanol

: 1374961-75-7
C₁₃H₁₄BrNO

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2012.03.016

Reference yield:

: 1374961-72-4
methyl 5-isopropyl-3-phenylisoxazole-4-carboxylate

: 1374961-75-7
C₁₃H₁₄BrNO

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

2: carbon tetrabromide; triphenylphosphine / dichloromethane / 20 °C

With carbon tetrabromide; diisobutylaluminium hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmc.2012.03.016

Reference yield:

: 100-52-7
benzaldehyde

: 1374961-75-7
C₁₃H₁₄BrNO

Guidance literature:: Multi-step reaction with 5 steps

1: hydroxylamine hydrochloride; sodium hydroxide / ethanol / 90 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 20 °C

3: sodium methylate; triethylamine / methanol / 20 °C

4: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

5: carbon tetrabromide; triphenylphosphine / dichloromethane / 20 °C

With N-chloro-succinimide; carbon tetrabromide; hydroxylamine hydrochloride; sodium methylate; diisobutylaluminium hydride; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.03.016