methyl N-[(2Z)-3-[4-(2-furyl)phenyl]-3-(3-thienyl)-2-propen-1-yl]-N-methylglycinate

Base Information

Chemical Name:methyl N-[(2Z)-3-[4-(2-furyl)phenyl]-3-(3-thienyl)-2-propen-1-yl]-N-methylglycinate
CAS No.:1018987-50-2
Molecular Formula:C₂₁H₂₁NO₃S
Molecular Weight:367.469
Hs Code.:

Synonyms:methyl N-[(2Z)-3-[4-(2-furyl)phenyl]-3-(3-thienyl)-2-propen-1-yl]-N-methylglycinate

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Chemical Property of methyl N-[(2Z)-3-[4-(2-furyl)phenyl]-3-(3-thienyl)-2-propen-1-yl]-N-methylglycinate

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Technology Process of methyl N-[(2Z)-3-[4-(2-furyl)phenyl]-3-(3-thienyl)-2-propen-1-yl]-N-methylglycinate

There total 7 articles about methyl N-[(2Z)-3-[4-(2-furyl)phenyl]-3-(3-thienyl)-2-propen-1-yl]-N-methylglycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₁₆O₃S₂

: 13515-93-0
N-methylglycine methyl ester hydrochloride

: 1018987-50-2
methyl N-[(2Z)-3-[4-(2-furyl)phenyl]-3-(3-thienyl)-2-propen-1-yl]-N-methylglycinate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 4 ℃;

Reference yield:

: C₁₈H₁₆O₄S₂

: 13515-93-0
N-methylglycine methyl ester hydrochloride

: 1018987-50-2
methyl N-[(2Z)-3-[4-(2-furyl)phenyl]-3-(3-thienyl)-2-propen-1-yl]-N-methylglycinate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 4 ℃;

Reference yield:

: 1018987-52-4
3-[4-(2-furyl)phenyl]-2-propyn-1-ol

: 1018987-50-2
methyl N-[(2Z)-3-[4-(2-furyl)phenyl]-3-(3-thienyl)-2-propen-1-yl]-N-methylglycinate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / 0.5 h / -20 - 0 °C

1.2: 0.5 h / -20 °C

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 60 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 - 5 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 °C

With potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; water;