N³-(3-(dimethylamino)propyl)-4-nitro-N¹-(pyridin-4-yl)benzene-1,3-diamine

Base Information

Chemical Name:N³-(3-(dimethylamino)propyl)-4-nitro-N¹-(pyridin-4-yl)benzene-1,3-diamine
CAS No.:1616475-68-3
Molecular Formula:C₁₆H₂₁N₅O₂
Molecular Weight:315.375
Hs Code.:

N<SUP>3</SUP>-(3-(dimethylamino)propyl)-4-nitro-N<SUP>1</SUP>-(pyridin-4-yl)benzene-1,3-diamine

Synonyms:N³-(3-(dimethylamino)propyl)-4-nitro-N¹-(pyridin-4-yl)benzene-1,3-diamine

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Chemical Property of N³-(3-(dimethylamino)propyl)-4-nitro-N¹-(pyridin-4-yl)benzene-1,3-diamine

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Technology Process of N³-(3-(dimethylamino)propyl)-4-nitro-N¹-(pyridin-4-yl)benzene-1,3-diamine

There total 3 articles about N³-(3-(dimethylamino)propyl)-4-nitro-N¹-(pyridin-4-yl)benzene-1,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 504-29-0
2-aminopyridine

: 92547-10-9
N¹-(5-chloro-2-nitrophenyl)-N³,N³-dimethylpropane-1,3-diamine

: 1616475-68-3
N³-(3-(dimethylamino)propyl)-4-nitro-N¹-(pyridin-4-yl)benzene-1,3-diamine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; for 20h; Inert atmosphere; Reflux;
DOI:10.1016/j.bmcl.2014.05.009

Reference yield:

: 109-55-7
1-amino-3-(dimethylamino)propane

: 1616475-68-3
N³-(3-(dimethylamino)propyl)-4-nitro-N¹-(pyridin-4-yl)benzene-1,3-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 24 h / Inert atmosphere; Reflux

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / 1,4-dioxane / 20 h / Inert atmosphere; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; acetonitrile;
DOI:10.1016/j.bmcl.2014.05.009

Reference yield:

: 611-06-3
2,4-dichloronitrobenzene

: 1616475-68-3
N³-(3-(dimethylamino)propyl)-4-nitro-N¹-(pyridin-4-yl)benzene-1,3-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 24 h / Inert atmosphere; Reflux

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / 1,4-dioxane / 20 h / Inert atmosphere; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; acetonitrile;
DOI:10.1016/j.bmcl.2014.05.009