C6H5B(μ-C3H3N2)2(μ-OBC6H5O)BC6H5

Base Information

Chemical Name:C6H5B(μ-C3H3N2)2(μ-OBC6H5O)BC6H5
CAS No.:99593-93-8
Molecular Formula:C₂₄H₂₁B₃N₄O₂
Molecular Weight:429.889
Hs Code.:

Synonyms:C6H5B(μ-C3H3N2)2(μ-OBC6H5O)BC6H5

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Chemical Property of C6H5B(μ-C3H3N2)2(μ-OBC6H5O)BC6H5

Chemical Property:

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Technology Process of C6H5B(μ-C3H3N2)2(μ-OBC6H5O)BC6H5

There total 4 articles about C6H5B(μ-C3H3N2)2(μ-OBC6H5O)BC6H5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 288-13-1
NH-pyrazole

: 98-80-6
phenylboronic acid

: 99593-93-8
C6H5B(μ-C3H3N2)2(μ-OBC6H5O)BC6H5

Guidance literature:: In benzene; byproducts: H2O; Ar atmosphere; azeotropic distn., solvent evapn. (vacuum), recrystn. (hexane);

Reference yield:

: 3262-89-3
triphenylboroxine

: 288-13-1
NH-pyrazole

: 99593-93-8
C6H5B(μ-C3H3N2)2(μ-OBC6H5O)BC6H5

Guidance literature:: In diethyl ether; standing for a few days at room temp.;

Reference yield:

: 67-56-1
methanol

: 115509-09-6,115509-06-3,109088-15-5
4,8-dichloro-4,8-diphenylpyrazabole

: 115419-91-5
4,8-dimethoxy-4,8-diphenylpyrazabole

: 99593-93-8
C6H5B(μ-C3H3N2)2(μ-OBC6H5O)BC6H5

Guidance literature:: In triethylamine; addn. of anhyd. MeOH to a soln. of PhClB(μ-pz)2BPhCl in anhyd. Et3N with cooling, vigorous reaction, stirring for 24 h at ambient temp., filtration, volatiles removed under vacuum;; washed with H2O, dried over P4O10, dissolved in boiling pentane/n-hexane, upon cooling to room temp. pptn. of one isomer A (colorless, m.p. 136-138°C, 60%); isomer A characterized by (1)H- and (11)B-NMR-spectra;;