(5S)-N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-tert-butyldiphenylsilyl-5-(N(3)-2-(trimethylsilyl)ethoxymethyl-3'-O-tert-butyldiphenylsilyl-thymidin-α(5)-yl)-5,6-dihydrothymidine

Base Information

Chemical Name:(5S)-N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-tert-butyldiphenylsilyl-5-(N(3)-2-(trimethylsilyl)ethoxymethyl-3'-O-tert-butyldiphenylsilyl-thymidin-α(5)-yl)-5,6-dihydrothymidine
CAS No.:1072452-76-6
Molecular Formula:C₆₄H₉₂N₄O₁₂Si₄
Molecular Weight:1221.8
Hs Code.:

(5S)-N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-tert-butyldiphenylsilyl-5-(N(3)-2-(trimethylsilyl)ethoxymethyl-3'-O-tert-butyldiphenylsilyl-thymidin-α(5)-yl)-5,6-dihydrothymidine

Synonyms:(5S)-N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-tert-butyldiphenylsilyl-5-(N(3)-2-(trimethylsilyl)ethoxymethyl-3'-O-tert-butyldiphenylsilyl-thymidin-α(5)-yl)-5,6-dihydrothymidine

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Chemical Property of (5S)-N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-tert-butyldiphenylsilyl-5-(N(3)-2-(trimethylsilyl)ethoxymethyl-3'-O-tert-butyldiphenylsilyl-thymidin-α(5)-yl)-5,6-dihydrothymidine

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Technology Process of (5S)-N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-tert-butyldiphenylsilyl-5-(N(3)-2-(trimethylsilyl)ethoxymethyl-3'-O-tert-butyldiphenylsilyl-thymidin-α(5)-yl)-5,6-dihydrothymidine

There total 1 articles about (5S)-N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-tert-butyldiphenylsilyl-5-(N(3)-2-(trimethylsilyl)ethoxymethyl-3'-O-tert-butyldiphenylsilyl-thymidin-α(5)-yl)-5,6-dihydrothymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 1181222-27-4
C₇₆H₁₂₀N₄O₁₂Si₆

: 1072452-77-7
(5R)-N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-tert-butyldiphenylsilyl-5-(N(3)-2-(trimethylsilyl)ethoxymethyl-3'-O-tert-butyldiphenylsilyl-thymidin-α(5)-yl)-5,6-dihydrothymidine

: 1072452-76-6
(5S)-N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-tert-butyldiphenylsilyl-5-(N(3)-2-(trimethylsilyl)ethoxymethyl-3'-O-tert-butyldiphenylsilyl-thymidin-α(5)-yl)-5,6-dihydrothymidine

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 20 ℃; for 4h;
DOI:10.1039/b810008j

Reference yield: 84.0%

: 1072452-76-6
(5S)-N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-tert-butyldiphenylsilyl-5-(N(3)-2-(trimethylsilyl)ethoxymethyl-3'-O-tert-butyldiphenylsilyl-thymidin-α(5)-yl)-5,6-dihydrothymidine

: 239808-67-4
4,4’-dimethoxytrityl trifluoromethanesulfonate

: (5S)-N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-tert-butyldiphenylsilyl-5-(N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-dimethoxytrityl-3'-O-tert-butyldiphenylsilyl-thymidin-α(5)-yl)-5,6-dihydrothymidine

Guidance literature:: 4,4'-dimethoxytrityl trifluoromethanesulfonate; With pyridine; at 20 ℃; for 3h; Molecular sieve;

(5S)-N(3)-2-(trimethylsilyl)ethoxymethyl-5'-O-tert-butyldiphenylsilyl-5-(N(3)-2-(trimethylsilyl)ethoxymethyl-3'-O-tert-butyldiphenylsilyl-thymidin-α(5)-yl)-5,6-dihydrothymidine; With pyridine; at 20 ℃; for 6h; Molecular sieve;
DOI:10.1039/b810008j