<1R-(1α,2α,3α)>-1-(4-morpholinylcarbonyl)-3-phenylcyclopropane-2-carboxaldehyde

Base Information

• Chemical Name: <1R-(1α,2α,3α)>-1-(4-morpholinylcarbonyl)-3-phenylcyclopropane-2-carboxaldehyde
• CAS No.: 140926-05-2
• Molecular Formula: C₁₅H₁₇NO₃
• Molecular Weight: 259.305

Synonyms:<1R-(1α,2α,3α)>-1-(4-morpholinylcarbonyl)-3-phenylcyclopropane-2-carboxaldehyde

Chemical Property of <1R-(1α,2α,3α)>-1-(4-morpholinylcarbonyl)-3-phenylcyclopropane-2-carboxaldehyde

Chemical Property:

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Technology Process of <1R-(1α,2α,3α)>-1-(4-morpholinylcarbonyl)-3-phenylcyclopropane-2-carboxaldehyde

There total 10 articles about <1R-(1α,2α,3α)>-1-(4-morpholinylcarbonyl)-3-phenylcyclopropane-2-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1-(4-morpholinylcarbonyl)-2-formyl-3-phenylcyclopropane (140926-05-2,141042-62-8,141506-51-6,141506-55-0,141506-57-2,141506-58-3) → 1-(4-morpholinylcarbonyl)-2-formyl-3-phenylcyclopropane (140926-05-2,141042-62-8,141506-51-6,141506-55-0,141506-57-2,141506-58-3)

Guidance literature:

With potassium carbonate; In methanol; for 24h; Ambient temperature;

DOI:10.1021/jm960059+

Reference yield: 82.0%

1-(4-morpholinylcarbonyl)-2-(hydroxymethyl)-3-phenylcyclopropane (130780-69-7,141041-95-4,141506-48-1,141506-56-1) → 1-(4-morpholinylcarbonyl)-2-formyl-3-phenylcyclopropane (140926-05-2,141042-62-8,141506-51-6,141506-55-0,141506-57-2,141506-58-3)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; for 48h; Ambient temperature;

DOI:10.1016/S0040-4039(00)97718-9

Reference yield: 68.0%

<1R-(1α,2α,3α)>-2-(hydroxymethyl)-1-(4-morpholinylcarbonyl)-3-phenylcyclopropane (141041-95-4) → <1R-(1α,2α,3α)>-1-(4-morpholinylcarbonyl)-3-phenylcyclopropane-2-carboxaldehyde (140926-05-2)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; for 48h; Ambient temperature;

DOI:10.1021/jm00088a005

upstream raw materials:

1-(4-morpholinylcarbonyl)-2-formyl-3-phenylcyclopropane

cis-3-phenyl-2-propen-1-yl diazoacetate

1-(4-morpholinylcarbonyl)-2-(hydroxymethyl)-3-phenylcyclopropane

(Z)-cinnamyl alcohol

Downstream raw materials:

(1S,2S,3R)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid

(2S,1'S,2'S,3'S)-2-(2'-carboxy-3'-phenylcyclopropyl)glycine

(2R,1'S,2'S,3'S)-2-(2'-carboxy-3'-phenylcyclopropyl)glycine

(2S,1'R,2'R,3'R)-2-(2'-carboxy-3'-phenylcyclopropyl)glycine

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