N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-oxocyclohex-1-enyl)ethyl]formamide

Base Information

• Chemical Name: N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-oxocyclohex-1-enyl)ethyl]formamide
• CAS No.: 363132-77-8
• Molecular Formula: C₁₇H₂₁NO₄
• Molecular Weight: 303.358

Synonyms:N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-oxocyclohex-1-enyl)ethyl]formamide

Chemical Property of N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-oxocyclohex-1-enyl)ethyl]formamide

Chemical Property:

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Technology Process of N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-oxocyclohex-1-enyl)ethyl]formamide

There total 1 articles about N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-oxocyclohex-1-enyl)ethyl]formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-methoxycyclohexa-1,4-dien-1-yl)ethyl]formamide (363132-72-3) → N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-oxocyclohex-1-enyl)ethyl]formamide (363132-77-8)

Guidance literature:

With formic acid; at 20 ℃;

DOI:10.1016/S0040-4020(01)00497-5

Reference yield: 76.3%

ethane-1,2-dithiol (540-63-6) + N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-oxocyclohex-1-enyl)ethyl]formamide (363132-77-8) → N-{2-(1,4-dithiaspiro[4.5]dec-7-en-8-yl)ethyl}-N-(3-hydroxy-4-methoxybenzyl)formamide (363132-86-9)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 14h;

DOI:10.1016/S0040-4020(01)00497-5

Reference yield: 69.0%

N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-oxocyclohex-1-enyl)ethyl]formamide (363132-77-8) → N-[2-(4-hydroxycyclohex-1-enyl)ethyl]-N-(3-hydroxy-4-methoxybenzyl)formamide

Guidance literature:

With sodium tetrahydroborate; In methanol; dichloromethane; at 20 ℃;

DOI:10.1016/S0040-4020(01)00497-5

upstream raw materials:

N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-methoxycyclohexa-1,4-dien-1-yl)ethyl]formamide

Downstream raw materials:

N-{2-(1,4-dithiaspiro[4.5]dec-7-en-8-yl)ethyl}-N-(3-hydroxy-4-methoxybenzyl)formamide

N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-aminocyclohex-1-enyl)ethyl]formamide

5-{[2-(1,4-dithiaspiro[4.5]dec-7-en-8-yl)ethylamino]methyl}-2-methoxyphenol

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