N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-methoxycyclohexa-1,4-dien-1-yl)ethyl]formamide

Base Information

• Chemical Name: N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-methoxycyclohexa-1,4-dien-1-yl)ethyl]formamide
• CAS No.: 363132-72-3
• Molecular Formula: C₁₈H₂₃NO₄
• Molecular Weight: 317.385

Synonyms:N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-methoxycyclohexa-1,4-dien-1-yl)ethyl]formamide

Chemical Property of N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-methoxycyclohexa-1,4-dien-1-yl)ethyl]formamide

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Technology Process of N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-methoxycyclohexa-1,4-dien-1-yl)ethyl]formamide

There total 1 articles about N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-methoxycyclohexa-1,4-dien-1-yl)ethyl]formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

phenyl formate (1864-94-4) + 2-methoxy-5-{[2-(4-methoxyphenyl)ethylamino]methyl}phenol (363132-68-7) → N-(2-cyclohex-1-enyl-ethyl)-N-(3-hydroxy-4-methoxybenzyl)formamide (363132-74-5) + N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-methoxycyclohexa-1,4-dien-1-yl)ethyl]formamide (363132-72-3)

Guidance literature:

2-methoxy-5-{[2-(4-methoxyphenyl)ethylamino]methyl}phenol; With lithium; In tetrahydrofuran; ammonia; tert-butyl alcohol; at -60 - -55 ℃; for 4h;

phenyl formate; In ethyl acetate; for 0.75h; Heating;

DOI:10.1016/S0040-4020(01)00497-5

Reference yield: 91.5%

ethylene glycol (107-21-1) + N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-methoxycyclohexa-1,4-dien-1-yl)ethyl]formamide (363132-72-3) → N-{2-(1,4-dioxaspiro[4.5]dec-7-en-8-yl)ethyl}-N-(3-hydroxy-4-methoxybenzyl)formamide

Guidance literature:

With methanesulfonic acid; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1016/S0040-4020(01)00497-5

Reference yield: 79.0%

N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-methoxycyclohexa-1,4-dien-1-yl)ethyl]formamide (363132-72-3) → N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-oxocyclohex-1-enyl)ethyl]formamide (363132-77-8)

Guidance literature:

With formic acid; at 20 ℃;

DOI:10.1016/S0040-4020(01)00497-5

upstream raw materials:

phenyl formate

2-methoxy-5-{[2-(4-methoxyphenyl)ethylamino]methyl}phenol

Downstream raw materials:

N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-oxocyclohex-1-enyl)ethyl]formamide

N-(3-hydroxy-4-methoxybenzyl)-N-[2-(4-aminocyclohex-1-enyl)ethyl]formamide

5-{[2-(1,4-dithiaspiro[4.5]dec-7-en-8-yl)ethylamino]methyl}-2-methoxyphenol

N-{2-(1,4-dithiaspiro[4.5]dec-7-en-8-yl)ethyl}-N-(3-hydroxy-4-methoxybenzyl)formamide

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