2,2,4,4,6,6-hexakis(2-methyl-1λ⁴-pyridin-1-yl)-1,3,5,2λ⁵,4λ⁵,6λ⁵-triazatriphosphinine

Base Information

• Chemical Name: 2,2,4,4,6,6-hexakis(2-methyl-1λ⁴-pyridin-1-yl)-1,3,5,2λ⁵,4λ⁵,6λ⁵-triazatriphosphinine
• CAS No.: 106424-55-9
• Molecular Formula: C₄₂H₄₈N₉P₃
• Molecular Weight: 771.825

Synonyms:2,2,4,4,6,6-hexakis(2-methyl-1λ⁴-pyridin-1-yl)-1,3,5,2λ⁵,4λ⁵,6λ⁵-triazatriphosphinine

Chemical Property of 2,2,4,4,6,6-hexakis(2-methyl-1λ⁴-pyridin-1-yl)-1,3,5,2λ⁵,4λ⁵,6λ⁵-triazatriphosphinine

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of 2,2,4,4,6,6-hexakis(2-methyl-1λ⁴-pyridin-1-yl)-1,3,5,2λ⁵,4λ⁵,6λ⁵-triazatriphosphinine

There total 2 articles about 2,2,4,4,6,6-hexakis(2-methyl-1λ⁴-pyridin-1-yl)-1,3,5,2λ⁵,4λ⁵,6λ⁵-triazatriphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

o-toluidine (95-53-4) → 2,2,4,4,6,6-hexakis(2-methyl-1λ4-pyridin-1-yl)-1,3,5,2λ5,4λ5,6λ5-triazatriphosphinine (106424-55-9)

Guidance literature:

With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; In neat (no solvent); for 2h; Microwave irradiation; Reflux;

DOI:10.1515/znb-2018-0136

Reference yield:

→ 2,2,4,4,6,6-hexakis(2-methyl-1λ4-pyridin-1-yl)-1,3,5,2λ5,4λ5,6λ5-triazatriphosphinine (106424-55-9)

Guidance literature:

Triphosphonitrilchlorid, o-Toluidin, 185 grad;

Reference yield: 53.0%

methanol (67-56-1) + 2,2,4,4,6,6-hexakis(2-methyl-1λ4-pyridin-1-yl)-1,3,5,2λ5,4λ5,6λ5-triazatriphosphinine (106424-55-9) → 2C42H48N9P3*H2O4S*2CH4O

Guidance literature:

With oxovanadium(IV) sulfate; for 4h; Reflux;

DOI:10.1016/j.molstruc.2020.127804

upstream raw materials:

o-toluidine

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