{3-[isobutoxycarbonyl-(4-methoxy-benzyl)-amino]-2-oxo-3-phenylsulfanyl-propyl}-(4-methoxy-benzyl)-carbamic acid isobutyl ester

Base Information

Chemical Name:{3-[isobutoxycarbonyl-(4-methoxy-benzyl)-amino]-2-oxo-3-phenylsulfanyl-propyl}-(4-methoxy-benzyl)-carbamic acid isobutyl ester
CAS No.:253591-07-0
Molecular Formula:C₃₅H₄₄N₂O₇S
Molecular Weight:636.81
Hs Code.:

Synonyms:{3-[isobutoxycarbonyl-(4-methoxy-benzyl)-amino]-2-oxo-3-phenylsulfanyl-propyl}-(4-methoxy-benzyl)-carbamic acid isobutyl ester

Suppliers and Price of {3-[isobutoxycarbonyl-(4-methoxy-benzyl)-amino]-2-oxo-3-phenylsulfanyl-propyl}-(4-methoxy-benzyl)-carbamic acid isobutyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of {3-[isobutoxycarbonyl-(4-methoxy-benzyl)-amino]-2-oxo-3-phenylsulfanyl-propyl}-(4-methoxy-benzyl)-carbamic acid isobutyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of {3-[isobutoxycarbonyl-(4-methoxy-benzyl)-amino]-2-oxo-3-phenylsulfanyl-propyl}-(4-methoxy-benzyl)-carbamic acid isobutyl ester

There total 5 articles about {3-[isobutoxycarbonyl-(4-methoxy-benzyl)-amino]-2-oxo-3-phenylsulfanyl-propyl}-(4-methoxy-benzyl)-carbamic acid isobutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1212-08-4
S-Phenyl benzenethiosulfonate

: 253590-88-4
{3-[isobutoxycarbonyl-(4-methoxy-benzyl)-amino]-2-oxo-propyl}-(4-methoxy-benzyl)-carbamic acid isobutyl ester

: 253591-07-0
{3-[isobutoxycarbonyl-(4-methoxy-benzyl)-amino]-2-oxo-3-phenylsulfanyl-propyl}-(4-methoxy-benzyl)-carbamic acid isobutyl ester

Guidance literature:: With n-butyllithium; In 1,2-dichloro-ethane; at -25 - 20 ℃; for 1h;
DOI:10.1016/S0223-5234(00)80031-8

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 253591-07-0
{3-[isobutoxycarbonyl-(4-methoxy-benzyl)-amino]-2-oxo-3-phenylsulfanyl-propyl}-(4-methoxy-benzyl)-carbamic acid isobutyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: Na₂SO₄ / CH₂Cl₂ / 20 °C

2: NaBH₄ / ethanol / 20 °C

3: 98 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

4: 90 percent / NaOCl; sat. NaHCO₃; KBr / TEMPO / CH₂Cl₂; H₂O / 0 - 20 °C

5: 44 percent / nBuLi / 1,2-dichloro-ethane / 1 h / -25 - 20 °C

With sodium hypochlorite; sodium tetrahydroborate; n-butyllithium; sodium hydrogencarbonate; sodium sulfate; triethylamine; potassium bromide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; In ethanol; dichloromethane; water; 1,2-dichloro-ethane; 1: Condensation / 2: Reduction / 3: Carboxylation / 4: Oxidation / 5: Substitution;
DOI:10.1016/S0223-5234(00)80031-8

Reference yield:

: 1,3-bis[(E)-(4-methoxybenzylidene)amino] propan-2-ol

: 253591-07-0
{3-[isobutoxycarbonyl-(4-methoxy-benzyl)-amino]-2-oxo-3-phenylsulfanyl-propyl}-(4-methoxy-benzyl)-carbamic acid isobutyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄ / ethanol / 20 °C

2: 98 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

3: 90 percent / NaOCl; sat. NaHCO₃; KBr / TEMPO / CH₂Cl₂; H₂O / 0 - 20 °C

4: 44 percent / nBuLi / 1,2-dichloro-ethane / 1 h / -25 - 20 °C

With sodium hypochlorite; sodium tetrahydroborate; n-butyllithium; sodium hydrogencarbonate; triethylamine; potassium bromide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; In ethanol; dichloromethane; water; 1,2-dichloro-ethane; 1: Reduction / 2: Carboxylation / 3: Oxidation / 4: Substitution;
DOI:10.1016/S0223-5234(00)80031-8